Benzyl-(6-formyl-3,5-dihydro-1H-thieno[3,4-c]pyrrol-4-carboxylat)-2,2-dioxid

Base Information

Chemical Name:Benzyl-(6-formyl-3,5-dihydro-1H-thieno[3,4-c]pyrrol-4-carboxylat)-2,2-dioxid
CAS No.:262611-68-7
Molecular Formula:C₁₅H₁₃NO₅S
Molecular Weight:319.338
Hs Code.:

Synonyms:Benzyl-(6-formyl-3,5-dihydro-1H-thieno[3,4-c]pyrrol-4-carboxylat)-2,2-dioxid

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Chemical Property of Benzyl-(6-formyl-3,5-dihydro-1H-thieno[3,4-c]pyrrol-4-carboxylat)-2,2-dioxid

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Technology Process of Benzyl-(6-formyl-3,5-dihydro-1H-thieno[3,4-c]pyrrol-4-carboxylat)-2,2-dioxid

There total 1 articles about Benzyl-(6-formyl-3,5-dihydro-1H-thieno[3,4-c]pyrrol-4-carboxylat)-2,2-dioxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 218628-86-5
3,5-Dihydro-1H-thieno[3,4-c]pyrrolcarbonsaeure-benzylester

: 262611-68-7
Benzyl-(6-formyl-3,5-dihydro-1H-thieno[3,4-c]pyrrol-4-carboxylat)-2,2-dioxid

Guidance literature:: With trichlorophosphate; at 90 ℃; for 1h;

Reference yield: 74.0%

: 79826-88-3
[ethyl-(14RS)-(14-cyano-12,13,14,17-tetrahydro-2,3,8,13,13,14-heptamethyl-15H-tripyrrin-1-carboxylato)]nickel(II)

: 557-34-6
zinc diacetate

: 262611-68-7
Benzyl-(6-formyl-3,5-dihydro-1H-thieno[3,4-c]pyrrol-4-carboxylat)-2,2-dioxid

: 262611-70-1
CH₃C(CN)C(CH₃)2CH₂C(NZn(NC(C(CH₃))2C))(CHC(NC(OCOCH₂C₆H₅)C₂)(CH₂)2SO₂)CHC(NC(C(CH₃))2CH)

Guidance literature:: With potassium hydroxide; In chloroform; 1.) Ni complex, 5N KOH, MeOH/H2O (9/1), THF, reflux, 45 min; 2.) the pyrrolaldehyde (1.8 equiv.), p-TsOH, CHCl3, reflux, 30 min; Zn acetate, NaOAc, ambient temp., 20 min.; chromy.;

Reference yield:

: C₂₅H₃₀N₄O₂^(2-)*Ni⁽²⁺⁾

: 262611-68-7
Benzyl-(6-formyl-3,5-dihydro-1H-thieno[3,4-c]pyrrol-4-carboxylat)-2,2-dioxid

: 6-[1-{5-[5-[5-Cyano-4,4,5-trimethyl-pyrrolidin-(2Z)-ylidenemethyl]-3,4-dimethyl-pyrrol-(2Z)-ylidenemethyl]-3,4-dimethyl-1H-pyrrol-2-yl}-meth-(Z)-ylidene]-2,2-dioxo-1,2,3,6-tetrahydro-2λ⁶-thieno[3,4-c]pyrrole-4-carboxylic acid benzyl ester

Guidance literature:: C₂₅H₃₀N₄O₂^(2-)*Ni⁽²⁺⁾; With potassium hydroxide; water; In tetrahydrofuran; methanol; for 0.75h; Heating;

Benzyl-(6-formyl-3,5-dihydro-1H-thieno[3,4-c]pyrrol-4-carboxylat)-2,2-dioxid; With toluene-4-sulfonic acid; In chloroform; for 0.5h; Heating;