<1S-(1α,2β,3α,4β,5β)>-1,5-Bis(methoxymethyl)-2,3,4-tris(phenylmethoxy)cyclopentane

Base Information

Chemical Name:<1S-(1α,2β,3α,4β,5β)>-1,5-Bis(methoxymethyl)-2,3,4-tris(phenylmethoxy)cyclopentane
CAS No.:106139-84-8
Molecular Formula:C₃₀H₃₆O₅
Molecular Weight:476.613
Hs Code.:

Synonyms:<1S-(1α,2β,3α,4β,5β)>-1,5-Bis(methoxymethyl)-2,3,4-tris(phenylmethoxy)cyclopentane

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Chemical Property of <1S-(1α,2β,3α,4β,5β)>-1,5-Bis(methoxymethyl)-2,3,4-tris(phenylmethoxy)cyclopentane

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Technology Process of <1S-(1α,2β,3α,4β,5β)>-1,5-Bis(methoxymethyl)-2,3,4-tris(phenylmethoxy)cyclopentane

There total 6 articles about <1S-(1α,2β,3α,4β,5β)>-1,5-Bis(methoxymethyl)-2,3,4-tris(phenylmethoxy)cyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 106139-80-4
<1S-(1α,2β,3α,4β,5α)>-2-(Methoxymethyl)-3,4,5-tris(phenylmethoxy)cyclopentanemethanol

: 74-88-4
methyl iodide

: 106139-84-8
<1S-(1α,2β,3α,4β,5β)>-1,5-Bis(methoxymethyl)-2,3,4-tris(phenylmethoxy)cyclopentane

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 1h; Ambient temperature;
DOI:10.1021/ja00187a031

Reference yield:

: 20770-84-7,113566-69-1,113566-70-4
2,3-di-O-benzyl-4,6-O-benzylidene-D-glucopyranose

: 106139-84-8
<1S-(1α,2β,3α,4β,5β)>-1,5-Bis(methoxymethyl)-2,3,4-tris(phenylmethoxy)cyclopentane

Guidance literature:: Multi-step reaction with 5 steps

2: 1,2-dichloro-ethane

3: Bu₃SnH, AIBN / toluene / Heating

4: LiAlH₄, AlCl₃

5: NaH

With lithium aluminium tetrahydride; aluminium trichloride; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydride; In 1,2-dichloro-ethane; toluene;
DOI:10.1021/ja00236a064

Reference yield:

: 119111-08-9,119111-09-0
(R)-1-O-Methyl-2-deoxy-3,4-bis-O-(phenylmethyl)-5,7-O-(phenylmethylene)-D-gluco-hept-1-enitol

: 106139-84-8
<1S-(1α,2β,3α,4β,5β)>-1,5-Bis(methoxymethyl)-2,3,4-tris(phenylmethoxy)cyclopentane

Guidance literature:: Multi-step reaction with 4 steps

1: 1,2-dichloro-ethane

2: Bu₃SnH, AIBN / toluene / Heating

3: LiAlH₄, AlCl₃

4: NaH

With lithium aluminium tetrahydride; aluminium trichloride; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydride; In 1,2-dichloro-ethane; toluene;
DOI:10.1021/ja00236a064