15-Benzyloxy-1-[(2R,5R,2'R,5'R)-5'-(tert-butyl-dimethyl-silanyloxymethyl)-octahydro-[2,2']bifuranyl-5-yl]-pentadecan-1-ol

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Chemical Name:15-Benzyloxy-1-[(2R,5R,2'R,5'R)-5'-(tert-butyl-dimethyl-silanyloxymethyl)-octahydro-[2,2']bifuranyl-5-yl]-pentadecan-1-ol
CAS No.:286853-83-6
Molecular Formula:C₃₇H₆₆O₅Si
Molecular Weight:619.014
Hs Code.:

Synonyms:15-Benzyloxy-1-[(2R,5R,2'R,5'R)-5'-(tert-butyl-dimethyl-silanyloxymethyl)-octahydro-[2,2']bifuranyl-5-yl]-pentadecan-1-ol

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Chemical Property of 15-Benzyloxy-1-[(2R,5R,2'R,5'R)-5'-(tert-butyl-dimethyl-silanyloxymethyl)-octahydro-[2,2']bifuranyl-5-yl]-pentadecan-1-ol

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Technology Process of 15-Benzyloxy-1-[(2R,5R,2'R,5'R)-5'-(tert-butyl-dimethyl-silanyloxymethyl)-octahydro-[2,2']bifuranyl-5-yl]-pentadecan-1-ol

There total 4 articles about 15-Benzyloxy-1-[(2R,5R,2'R,5'R)-5'-(tert-butyl-dimethyl-silanyloxymethyl)-octahydro-[2,2']bifuranyl-5-yl]-pentadecan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 286853-90-5
(2'R,2''R,5'R, 5R'')-[5'-(5''-(tert-butyldimethylsilyloxy)methyltetrahydrofuran-2''-yl)tetrahydrofuran-2'-yl]carbaldehyde

: C₂₁H₃₅BrMgO

: 286853-83-6
15-Benzyloxy-1-[(2R,5R,2'R,5'R)-5'-(tert-butyl-dimethyl-silanyloxymethyl)-octahydro-[2,2']bifuranyl-5-yl]-pentadecan-1-ol

Guidance literature:: DOI:10.1016/S0040-4039(99)01225-3

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 286853-83-6
15-Benzyloxy-1-[(2R,5R,2'R,5'R)-5'-(tert-butyl-dimethyl-silanyloxymethyl)-octahydro-[2,2']bifuranyl-5-yl]-pentadecan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole

3: 76 percent

With 1H-imidazole; 1: Silylation / 2: Oxidation / 3: Grignard reaction;
DOI:10.1016/S0040-4039(99)01225-3

Reference yield:

: 250138-82-0
(2R,2R',5R, 5R')-5,5'-bis(hydroxymethyl)octahydro-2,2'-bifuran

: 286853-83-6
15-Benzyloxy-1-[(2R,5R,2'R,5'R)-5'-(tert-butyl-dimethyl-silanyloxymethyl)-octahydro-[2,2']bifuranyl-5-yl]-pentadecan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole

3: 76 percent

With 1H-imidazole; 1: Silylation / 2: Oxidation / 3: Grignard reaction;
DOI:10.1016/S0040-4039(99)01225-3