(2S,3R)-3-[2-(5-benzyloxypyridyl)]-3-tert-butyldimethylsilyloxy-2-methylpropanal

Base Information

Chemical Name:(2S,3R)-3-[2-(5-benzyloxypyridyl)]-3-tert-butyldimethylsilyloxy-2-methylpropanal
CAS No.:909913-30-0
Molecular Formula:C₂₂H₃₁NO₃Si
Molecular Weight:385.579
Hs Code.:

Synonyms:(2S,3R)-3-[2-(5-benzyloxypyridyl)]-3-tert-butyldimethylsilyloxy-2-methylpropanal

Suppliers and Price of (2S,3R)-3-[2-(5-benzyloxypyridyl)]-3-tert-butyldimethylsilyloxy-2-methylpropanal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S,3R)-3-[2-(5-benzyloxypyridyl)]-3-tert-butyldimethylsilyloxy-2-methylpropanal

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S,3R)-3-[2-(5-benzyloxypyridyl)]-3-tert-butyldimethylsilyloxy-2-methylpropanal

There total 4 articles about (2S,3R)-3-[2-(5-benzyloxypyridyl)]-3-tert-butyldimethylsilyloxy-2-methylpropanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 909913-29-7
(2R,3R)-3-[2-(5-benzyloxypyridyl)]-3-tert-butyldimethylsilyloxy-2-methyl-1-propanol

: 909913-30-0
(2S,3R)-3-[2-(5-benzyloxypyridyl)]-3-tert-butyldimethylsilyloxy-2-methylpropanal

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 10h;
DOI:10.1016/j.tetasy.2006.06.010

Reference yield:

: 909913-42-4
(2R,3R)-1-acetoxy-3-[2-(5-benzyloxypyridyl)]-2-methyl-3-propanol

: 909913-30-0
(2S,3R)-3-[2-(5-benzyloxypyridyl)]-3-tert-butyldimethylsilyloxy-2-methylpropanal

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / imidazole / dimethylformamide / 12 h / 20 °C

2: 92 percent / potassium carbonate / methanol / 2 h / 20 °C

3: 42 percent / PCC / CH₂Cl₂ / 10 h / 20 °C

With 1H-imidazole; potassium carbonate; pyridinium chlorochromate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2006.06.010

Reference yield:

: 909913-28-6
(2R,3R)-1-acetoxy-3-[2-(5-benzyloxypyridyl)]-3-tert-butyldimethylsilyloxy-2-methyl-3-propanol

: 909913-30-0
(2S,3R)-3-[2-(5-benzyloxypyridyl)]-3-tert-butyldimethylsilyloxy-2-methylpropanal

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / potassium carbonate / methanol / 2 h / 20 °C

2: 42 percent / PCC / CH₂Cl₂ / 10 h / 20 °C

With potassium carbonate; pyridinium chlorochromate; In methanol; dichloromethane;
DOI:10.1016/j.tetasy.2006.06.010