6-chloro-7,8-dimethoxy-1-(3-methoxyphenyl)-2,3,4,5-tetrahydro-1H-3-benzazepine

Base Information

Chemical Name:6-chloro-7,8-dimethoxy-1-(3-methoxyphenyl)-2,3,4,5-tetrahydro-1H-3-benzazepine
CAS No.:100166-79-8
Molecular Formula:C₁₉H₂₂ClNO₃
Molecular Weight:347.842
Hs Code.:

Synonyms:6-chloro-7,8-dimethoxy-1-(3-methoxyphenyl)-2,3,4,5-tetrahydro-1H-3-benzazepine

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Chemical Property of 6-chloro-7,8-dimethoxy-1-(3-methoxyphenyl)-2,3,4,5-tetrahydro-1H-3-benzazepine

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Technology Process of 6-chloro-7,8-dimethoxy-1-(3-methoxyphenyl)-2,3,4,5-tetrahydro-1H-3-benzazepine

There total 4 articles about 6-chloro-7,8-dimethoxy-1-(3-methoxyphenyl)-2,3,4,5-tetrahydro-1H-3-benzazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 67287-60-9
N-[2-(2-chloro-3,4-dimethoxyphenyl)-ethyl]-2-hydroxy-2-(m-methoxyphenyl)ethylamine

: 100166-79-8
6-chloro-7,8-dimethoxy-1-(3-methoxyphenyl)-2,3,4,5-tetrahydro-1H-3-benzazepine

Guidance literature:: With sulfuric acid; trifluoroacetic acid; for 3h; Heating;
DOI:10.1021/jm00155a024

Reference yield:

: 32017-77-9,53631-49-5
2-(m-methoxyphenyl)oxirane

: 100166-79-8
6-chloro-7,8-dimethoxy-1-(3-methoxyphenyl)-2,3,4,5-tetrahydro-1H-3-benzazepine

Guidance literature:: Multi-step reaction with 2 steps

1: 38 percent / tetrahydrofuran / 16 h / Heating

2: 91 percent / trifluoroacetic acid, conc. aq. H₂SO₄ / 3 h / Heating

With sulfuric acid; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1021/jm00155a024

Reference yield:

: 67287-36-9
2-(2-chloro-3,4-dimethoxyphenyl)ethylamine

: 100166-79-8
6-chloro-7,8-dimethoxy-1-(3-methoxyphenyl)-2,3,4,5-tetrahydro-1H-3-benzazepine

Guidance literature:: Multi-step reaction with 2 steps

1: 38 percent / tetrahydrofuran / 16 h / Heating

2: 91 percent / trifluoroacetic acid, conc. aq. H₂SO₄ / 3 h / Heating

With sulfuric acid; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1021/jm00155a024