1,3-di-(3-methylphenyl)-1,3-dihydro-4,5-dioxo-2-thioxofuro<2,3-d>pyrimidine

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Chemical Name:1,3-di-(3-methylphenyl)-1,3-dihydro-4,5-dioxo-2-thioxofuro<2,3-d>pyrimidine
CAS No.:135764-10-2
Molecular Formula:C₂₀H₁₆N₂O₃S
Molecular Weight:364.425
Hs Code.:

Synonyms:1,3-di-(3-methylphenyl)-1,3-dihydro-4,5-dioxo-2-thioxofuro<2,3-d>pyrimidine

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Chemical Property of 1,3-di-(3-methylphenyl)-1,3-dihydro-4,5-dioxo-2-thioxofuro<2,3-d>pyrimidine

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Technology Process of 1,3-di-(3-methylphenyl)-1,3-dihydro-4,5-dioxo-2-thioxofuro<2,3-d>pyrimidine

There total 3 articles about 1,3-di-(3-methylphenyl)-1,3-dihydro-4,5-dioxo-2-thioxofuro<2,3-d>pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 135764-06-6
1,3-di-(3-methylphenyl)-1,3-dihydro-2-thioxo-5-chloroacetylpyrimidine

: 135764-10-2
1,3-di-(3-methylphenyl)-1,3-dihydro-4,5-dioxo-2-thioxofuro<2,3-d>pyrimidine

Guidance literature:: With sodium acetate; In ethanol; for 0.5h; Heating;

Reference yield: 88.0%

: 128721-46-0
1,3-di(3-methylphenyl)-2-thiobarbituric acid

: 79-04-9
chloroacetyl chloride

: 135764-10-2
1,3-di-(3-methylphenyl)-1,3-dihydro-4,5-dioxo-2-thioxofuro<2,3-d>pyrimidine

Guidance literature:: With aluminum oxide; at 90 - 100 ℃; for 0.0833333h; microwave irradiation;

Reference yield:

: 128721-46-0
1,3-di(3-methylphenyl)-2-thiobarbituric acid

: 135764-10-2
1,3-di-(3-methylphenyl)-1,3-dihydro-4,5-dioxo-2-thioxofuro<2,3-d>pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / K₂CO₃ / 0.03 h / 90 - 100 °C / microwave irradiation

2: 93 percent / K₂CO₃ / 0.07 h / 90 - 100 °C / microwave irradiation

With potassium carbonate;