C₅₀H₅₆Si₂

Base Information

Chemical Name:C₅₀H₅₆Si₂
CAS No.:214628-17-8
Molecular Formula:C₅₀H₅₆Si₂
Molecular Weight:713.166
Hs Code.:

C<sub>50</sub>H<sub>56</sub>Si<sub>2</sub>

Synonyms:C₅₀H₅₆Si₂

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Chemical Property of C₅₀H₅₆Si₂

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Technology Process of C₅₀H₅₆Si₂

There total 5 articles about C₅₀H₅₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 214628-16-7
1-(triisopropylsilyl)ethynyl-2-[(E)-6-(trimethylsilyl)hex-3-ene-1,5-diynyl]benzene

: 214628-08-7
N,N-tetramethylene-N'-(2-iodophenyl)triazene

: 214628-17-8
C₅₀H₅₆Si₂

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; potassium hydroxide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In tetrahydrofuran; water;
DOI:10.1016/S0040-4039(98)01583-4

Reference yield:

: 335378-29-5
2-ethynyl-1-[(triisopropylsilyl)ethynyl]benzene

: 214628-17-8
C₅₀H₅₆Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / Pd(PPh₃)2; CuI / triethylamine; tetrahydrofuran / 60 °C

2: 27 percent / aq. KOH / PdCl₂(PPh₃)2; CuI / tetrahydrofuran; triethylamine / 60 °C

With potassium hydroxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; bis(triphenylphosphine)palladium⁽⁰⁾; In tetrahydrofuran; triethylamine;
DOI:10.1002/1099-0690(200109)2001:18<3485::AID-EJOC3485>3.0.CO;2-I

Reference yield:

: 188003-93-2
triisopropyl((2-((trimethylsilyl)ethynyl) phenyl)ethynyl)silane

: 214628-17-8
C₅₀H₅₆Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / K₂CO₃ / methanol; diethyl ether; tetrahydrofuran / 2 h

2: 65 percent / Pd(PPh₃)2; CuI / triethylamine; tetrahydrofuran / 60 °C

3: 27 percent / aq. KOH / PdCl₂(PPh₃)2; CuI / tetrahydrofuran; triethylamine / 60 °C

With potassium hydroxide; potassium carbonate; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; bis(triphenylphosphine)palladium⁽⁰⁾; In tetrahydrofuran; methanol; diethyl ether; triethylamine;
DOI:10.1002/1099-0690(200109)2001:18<3485::AID-EJOC3485>3.0.CO;2-I