1-(4-(4-(2-methoxyphenyl)piperazin-1-yl)butyl)-3-methyl-5,5-diphenylimidazolidine-2,4-dione hydrochloride

Base Information

Chemical Name:1-(4-(4-(2-methoxyphenyl)piperazin-1-yl)butyl)-3-methyl-5,5-diphenylimidazolidine-2,4-dione hydrochloride
CAS No.:1370333-48-4
Molecular Formula:C₃₁H₃₆N₄O₃*ClH
Molecular Weight:549.113
Hs Code.:

Synonyms:1-(4-(4-(2-methoxyphenyl)piperazin-1-yl)butyl)-3-methyl-5,5-diphenylimidazolidine-2,4-dione hydrochloride

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Chemical Property of 1-(4-(4-(2-methoxyphenyl)piperazin-1-yl)butyl)-3-methyl-5,5-diphenylimidazolidine-2,4-dione hydrochloride

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Technology Process of 1-(4-(4-(2-methoxyphenyl)piperazin-1-yl)butyl)-3-methyl-5,5-diphenylimidazolidine-2,4-dione hydrochloride

There total 2 articles about 1-(4-(4-(2-methoxyphenyl)piperazin-1-yl)butyl)-3-methyl-5,5-diphenylimidazolidine-2,4-dione hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 35386-24-4
1-(2-Methoxyphenyl)piperazine

: 1370333-39-3
1-(4-bromobutyl)-3-methyl-5,5-diphenylimidazolidine-2,4-dione

: 1370333-48-4
1-(4-(4-(2-methoxyphenyl)piperazin-1-yl)butyl)-3-methyl-5,5-diphenylimidazolidine-2,4-dione hydrochloride

Guidance literature:: 1-(2-Methoxyphenyl)piperazine; With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; In acetone; for 0.5h; Reflux;

1-(4-bromobutyl)-3-methyl-5,5-diphenylimidazolidine-2,4-dione; In acetone; at 20 ℃; for 72h;

With hydrogenchloride; In methanol;
DOI:10.1016/j.bmc.2012.02.009

Reference yield:

: 4224-00-4
3-methyl-5,5-diphenyl-imidazolidine-2,4-dione

: 1370333-48-4
1-(4-(4-(2-methoxyphenyl)piperazin-1-yl)butyl)-3-methyl-5,5-diphenylimidazolidine-2,4-dione hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate / acetone / 0.25 h / 40 - 45 °C / Microwave irradiation

1.2: 2.5 h / 40 - 60 °C / Microwave irradiation

2.1: N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate / acetone / 0.5 h / Reflux

2.2: 72 h / 20 °C

With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; In acetone;
DOI:10.1016/j.bmc.2012.02.009