6-methoxy-2-methyl-7-(propan-2-yloxy)-3-(3,4,5-trimethoxybenzoyl)-1-benzofuran

Base Information

Chemical Name:6-methoxy-2-methyl-7-(propan-2-yloxy)-3-(3,4,5-trimethoxybenzoyl)-1-benzofuran
CAS No.:945772-41-8
Molecular Formula:C₂₃H₂₆O₇
Molecular Weight:414.455
Hs Code.:

Synonyms:6-methoxy-2-methyl-7-(propan-2-yloxy)-3-(3,4,5-trimethoxybenzoyl)-1-benzofuran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-methoxy-2-methyl-7-(propan-2-yloxy)-3-(3,4,5-trimethoxybenzoyl)-1-benzofuran

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Technology Process of 6-methoxy-2-methyl-7-(propan-2-yloxy)-3-(3,4,5-trimethoxybenzoyl)-1-benzofuran

There total 9 articles about 6-methoxy-2-methyl-7-(propan-2-yloxy)-3-(3,4,5-trimethoxybenzoyl)-1-benzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: (E)-3-(2-isopropyl-3-methoxy-6-iodophenyl)-1-(3,4,5-trimethoxy)-but-2-ene-1-one

: 945772-41-8
6-methoxy-2-methyl-7-(propan-2-yloxy)-3-(3,4,5-trimethoxybenzoyl)-1-benzofuran

Guidance literature:: With triethylsilane; 2,2'-azobis(2-methylpropionamidine) dihydrochloride; In tetrahydrofuran; at 85 ℃; for 15h; Inert atmosphere;

Reference yield: 48.0%

: 25245-29-8
5-iodo-1,2,3-trimethoxybenzene

: 905751-80-6
2-isopropoxy-3-methoxy-6-iodophenol

: 201230-82-2
carbon monoxide

: 16466-97-0,13254-27-8
1-propynylmagnesium bromide

: 945772-41-8
6-methoxy-2-methyl-7-(propan-2-yloxy)-3-(3,4,5-trimethoxybenzoyl)-1-benzofuran

Guidance literature:: 2-isopropoxy-3-methoxy-6-iodophenol; 1-propynylmagnesium bromide; With bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; at 16 ℃; Inert atmosphere; Industry scale; Reflux;

5-iodo-1,2,3-trimethoxybenzene; carbon monoxide; In dimethyl sulfoxide; at 30 ℃; for 39h; under 51.7162 - 206.865 Torr; Inert atmosphere; Industry scale;

With tributylphosphine; In dimethyl sulfoxide; at 30 ℃; for 0.5h; Product distribution / selectivity; Inert atmosphere; Industry scale;

Reference yield:

: 25245-29-8
5-iodo-1,2,3-trimethoxybenzene

: C₁₃H₁₆O₃

: 201230-82-2
carbon monoxide

: 945772-41-8
6-methoxy-2-methyl-7-(propan-2-yloxy)-3-(3,4,5-trimethoxybenzoyl)-1-benzofuran

Guidance literature:: 5-iodo-1,2,3-trimethoxybenzene; C₁₃H₁₆O₃; carbon monoxide; In dimethyl sulfoxide; at 90 ℃; for 17h;

With ammonium chloride; In water; dimethyl sulfoxide;