Technology Process of C40H30NO12P
There total 7 articles about C40H30NO12P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
chloroform;
at 20 ℃;
for 2h;
DOI:10.1002/chem.200390167
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Et3N; 1H-tetrazole / CHCl3 / 0.5 h / 20 °C
2: 400 mg / mCPBA / CHCl3 / 0.5 h / 20 °C
3: 96 percent / EDC*HCl / CHCl3 / 2 h / 20 °C
With
1H-tetrazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
chloroform;
DOI:10.1002/chem.200390167
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 52 percent / H2SO4 / Heating
2: Cs2CO3 / dimethylformamide / 0.33 h / 20 °C
3: 110 mg / aq. NaOH / methanol / 1 h / 20 °C
4: Et3N; 1H-tetrazole / CHCl3 / 0.5 h / 20 °C
5: 400 mg / mCPBA / CHCl3 / 0.5 h / 20 °C
6: 96 percent / EDC*HCl / CHCl3 / 2 h / 20 °C
With
1H-tetrazole; sodium hydroxide; sulfuric acid; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/chem.200390167