C₂₆H₃₀N₂O₃

Base Information

Chemical Name:C₂₆H₃₀N₂O₃
CAS No.:1416772-56-9
Molecular Formula:C₂₆H₃₀N₂O₃
Molecular Weight:418.536
Hs Code.:

C<sub>26</sub>H<sub>30</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₆H₃₀N₂O₃

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Chemical Property of C₂₆H₃₀N₂O₃

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Technology Process of C₂₆H₃₀N₂O₃

There total 14 articles about C₂₆H₃₀N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1416772-46-7
(2R,3S,4S)-4-(dibenzylamino)-3-hydroxy-2-methyl-5-(pyridin-3-yl)pentanoic acid

: 18107-18-1
diazomethyl-trimethyl-silane

: 1416772-56-9
C₂₆H₃₀N₂O₃

Guidance literature:: In methanol; diethyl ether; toluene; at 0 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ml300385q

Reference yield:

: 115167-43-6
methyl (Z)-2-acetamido-3-(3-pyridyl)propenoate

: 1416772-56-9
C₂₆H₃₀N₂O₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetrafluoroboric acid; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen / methanol / 18 h / 50 °C / 3750.38 Torr / Autoclave; Schlenk technique

2.1: thionyl chloride / methanol / 18 h / 0 - 80 °C / Inert atmosphere; Schlenk technique

3.1: sodium cyanoborohydride; acetic acid / methanol / 24 h / 20 °C / Molecular sieve; Inert atmosphere; Schlenk technique

4.1: lithium aluminium tetrahydride / diethyl ether / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

5.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

6.1: chromium dichloride / tetrahydrofuran / 0.42 h / 200 °C / Inert atmosphere; Schlenk technique

6.2: 3 h / 20 °C

7.1: AD-mix-α; methanesulfonamide / water; tert-butyl alcohol / 72 h / 20 °C / Inert atmosphere; Schlenk technique

8.1: sodium periodate / dichloromethane; water / 2 h / 20 °C / Inert atmosphere; Schlenk technique

9.1: 2,3-Dimethyl-2-butene; sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 0.75 h / 20 °C / Inert atmosphere; Schlenk technique

10.1: methanol; diethyl ether; toluene / 0.08 h / 0 °C / Inert atmosphere; Schlenk technique

With chromium dichloride; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; lithium aluminium tetrahydride; tetrafluoroboric acid; thionyl chloride; 2,3-Dimethyl-2-butene; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; methanesulfonamide; AD-mix-α; hydrogen; sodium cyanoborohydride; Dess-Martin periodane; acetic acid; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene; tert-butyl alcohol;
DOI:10.1021/ml300385q

Reference yield:

: 89890-92-6
N-acetyl-(β-3-pyridyl)-α,β-dehydroalanine

: 1416772-56-9
C₂₆H₃₀N₂O₃

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium acetate / 72 h / 20 °C / Inert atmosphere; Schlenk technique

2.1: tetrafluoroboric acid; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen / methanol / 18 h / 50 °C / 3750.38 Torr / Autoclave; Schlenk technique

3.1: thionyl chloride / methanol / 18 h / 0 - 80 °C / Inert atmosphere; Schlenk technique

4.1: sodium cyanoborohydride; acetic acid / methanol / 24 h / 20 °C / Molecular sieve; Inert atmosphere; Schlenk technique

5.1: lithium aluminium tetrahydride / diethyl ether / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

6.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

7.1: chromium dichloride / tetrahydrofuran / 0.42 h / 200 °C / Inert atmosphere; Schlenk technique

7.2: 3 h / 20 °C

8.1: AD-mix-α; methanesulfonamide / water; tert-butyl alcohol / 72 h / 20 °C / Inert atmosphere; Schlenk technique

9.1: sodium periodate / dichloromethane; water / 2 h / 20 °C / Inert atmosphere; Schlenk technique

10.1: 2,3-Dimethyl-2-butene; sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 0.75 h / 20 °C / Inert atmosphere; Schlenk technique

11.1: methanol; diethyl ether; toluene / 0.08 h / 0 °C / Inert atmosphere; Schlenk technique

With chromium dichloride; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; lithium aluminium tetrahydride; tetrafluoroboric acid; thionyl chloride; 2,3-Dimethyl-2-butene; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; methanesulfonamide; AD-mix-α; hydrogen; sodium acetate; sodium cyanoborohydride; Dess-Martin periodane; acetic acid; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene; tert-butyl alcohol;
DOI:10.1021/ml300385q