(R)-3-(2-(benzyloxy)-5-(benzyloxy(methyl-d2))phenyl)-3-phenylpropanoyl chloride

Base Information

Chemical Name:(R)-3-(2-(benzyloxy)-5-(benzyloxy(methyl-d2))phenyl)-3-phenylpropanoyl chloride
CAS No.:1191280-68-8
Molecular Formula:C₃₀H₂₇ClO₃
Molecular Weight:472.98
Hs Code.:

Synonyms:(R)-3-(2-(benzyloxy)-5-(benzyloxy(methyl-d2))phenyl)-3-phenylpropanoyl chloride

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Chemical Property of (R)-3-(2-(benzyloxy)-5-(benzyloxy(methyl-d2))phenyl)-3-phenylpropanoyl chloride

Chemical Property:

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Technology Process of (R)-3-(2-(benzyloxy)-5-(benzyloxy(methyl-d2))phenyl)-3-phenylpropanoyl chloride

There total 6 articles about (R)-3-(2-(benzyloxy)-5-(benzyloxy(methyl-d2))phenyl)-3-phenylpropanoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1191280-67-7
(R)-3-(2-(benzyloxy)-5-(benzyloxy(methyl-d2))phenyl)-3-phenylpropanoic acid

: 1191280-68-8
(R)-3-(2-(benzyloxy)-5-(benzyloxy(methyl-d2))phenyl)-3-phenylpropanoyl chloride

Guidance literature:: With pyridine; thionyl chloride; In toluene; for 1h; Reflux;

Reference yield:

: 100-39-0
benzyl bromide

: 1191280-68-8
(R)-3-(2-(benzyloxy)-5-(benzyloxy(methyl-d2))phenyl)-3-phenylpropanoyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / acetone / 5 h

2.1: iodine; magnesium / tetrahydrofuran / 1 h / 80 °C

2.2: 1 h / -30 °C

2.3: -30 - 20 °C

3.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 4 h / 20 °C

3.2: pH 2

4.1: pyridine; thionyl chloride / toluene / 1 h / Reflux

With pyridine; thionyl chloride; dihydrogen peroxide; iodine; potassium carbonate; magnesium; lithium hydroxide; In tetrahydrofuran; water; acetone; toluene;

Reference yield:

: 628711-07-9
benzyl 4-(benzyloxy)-3-bromobenzoate

: 1191280-68-8
(R)-3-(2-(benzyloxy)-5-(benzyloxy(methyl-d2))phenyl)-3-phenylpropanoyl chloride

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium aluminium deuteride / tetrahydrofuran / 12 h / 20 °C

2.1: potassium carbonate / acetone / 5 h

3.1: iodine; magnesium / tetrahydrofuran / 1 h / 80 °C

3.2: 1 h / -30 °C

3.3: -30 - 20 °C

4.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 4 h / 20 °C

4.2: pH 2

5.1: pyridine; thionyl chloride / toluene / 1 h / Reflux

With pyridine; thionyl chloride; lithium aluminium deuteride; dihydrogen peroxide; iodine; potassium carbonate; magnesium; lithium hydroxide; In tetrahydrofuran; water; acetone; toluene;