methyl 3,4,6-tri-O-benzyl-2-deoxy-1-(2-thiazolyl)-α-D-arabino-hexopyranoside

Base Information

Chemical Name:methyl 3,4,6-tri-O-benzyl-2-deoxy-1-(2-thiazolyl)-α-D-arabino-hexopyranoside
CAS No.:154796-55-1
Molecular Formula:C₃₁H₃₃NO₅S
Molecular Weight:531.673
Hs Code.:

Synonyms:methyl 3,4,6-tri-O-benzyl-2-deoxy-1-(2-thiazolyl)-α-D-arabino-hexopyranoside

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Chemical Property of methyl 3,4,6-tri-O-benzyl-2-deoxy-1-(2-thiazolyl)-α-D-arabino-hexopyranoside

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Technology Process of methyl 3,4,6-tri-O-benzyl-2-deoxy-1-(2-thiazolyl)-α-D-arabino-hexopyranoside

There total 9 articles about methyl 3,4,6-tri-O-benzyl-2-deoxy-1-(2-thiazolyl)-α-D-arabino-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 100-39-0
benzyl bromide

: 154796-58-4
methyl 3,4-di-O-benzyl-2-deoxy-1-(2-thiazolyl)-α-D-arabino-hexopyranoside

: 154796-55-1
methyl 3,4,6-tri-O-benzyl-2-deoxy-1-(2-thiazolyl)-α-D-arabino-hexopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 0.5h; Ambient temperature;

Reference yield: 100.0%

: 100-39-0
benzyl bromide

: 154796-54-0
methyl 3,4-di-O-benzyl-2-deoxy-1-(2-thiazolyl)-α-D-arabino-hexopyranoside

: 154796-55-1
methyl 3,4,6-tri-O-benzyl-2-deoxy-1-(2-thiazolyl)-α-D-arabino-hexopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 0.5h; Ambient temperature;

Reference yield:

: 3292-77-1
2-bromo-1-thiazol-2-yl-ethanone

: 154796-55-1
methyl 3,4,6-tri-O-benzyl-2-deoxy-1-(2-thiazolyl)-α-D-arabino-hexopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 95 percent / toluene / 3 h / Ambient temperature

2: 95 percent / 1N aq. NaOH / 0.5 h

3: 82 percent / CHCl₃ / 48 h / Heating

4: 18 percent / tetrahydrofuran / 5 h / -50 °C

5: 98 percent / HCl / 16 h / Ambient temperature

6: 100 percent / NaH / dimethylformamide / 0.5 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; sodium hydride; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide; toluene;