Technology Process of trans-4-(2-iodovinyl)-1,2-dimethoxybenzene
There total 5 articles about trans-4-(2-iodovinyl)-1,2-dimethoxybenzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(I) oxide; L-proline; potassium iodide;
In
ethanol;
at 110 ℃;
for 24h;
diastereospecific reaction;
Schlenk technique;
Sealed tube;
Inert atmosphere;
Green chemistry;
DOI:10.1055/s-0036-1588988
- Guidance literature:
-
With
N-iodo-succinimide; lithium acetate;
In
water; acetonitrile;
at 20 ℃;
for 1h;
DOI:10.1016/j.tet.2015.09.003
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium bromide; sodium molybdate dihydrate; dihydrogen peroxide / water / 25 °C
2: potassium iodide; copper(I) oxide; L-proline / ethanol / 24 h / 110 °C / Schlenk technique; Sealed tube; Inert atmosphere; Green chemistry
With
copper(I) oxide; sodium molybdate dihydrate; dihydrogen peroxide; L-proline; potassium iodide; potassium bromide;
In
ethanol; water;
2: |Finkelstein Reaction;
DOI:10.1055/s-0036-1588988
