[(S)-5-[(S)-3-tert-Butoxy-2-(11-imidazol-1-yl-undecanoylamino)-propionylamino]-5-(2-cyclohexyl-ethylcarbamoyl)-pentyl]-carbamic acid tert-butyl ester

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Chemical Name:[(S)-5-[(S)-3-tert-Butoxy-2-(11-imidazol-1-yl-undecanoylamino)-propionylamino]-5-(2-cyclohexyl-ethylcarbamoyl)-pentyl]-carbamic acid tert-butyl ester
CAS No.:1026800-59-8
Molecular Formula:C₄₀H₇₂N₆O₆
Molecular Weight:733.048
Hs Code.:

[(S)-5-[(S)-3-tert-Butoxy-2-(11-imidazol-1-yl-undecanoylamino)-propionylamino]-5-(2-cyclohexyl-ethylcarbamoyl)-pentyl]-carbamic acid tert-butyl ester

Synonyms:[(S)-5-[(S)-3-tert-Butoxy-2-(11-imidazol-1-yl-undecanoylamino)-propionylamino]-5-(2-cyclohexyl-ethylcarbamoyl)-pentyl]-carbamic acid tert-butyl ester

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Chemical Property of [(S)-5-[(S)-3-tert-Butoxy-2-(11-imidazol-1-yl-undecanoylamino)-propionylamino]-5-(2-cyclohexyl-ethylcarbamoyl)-pentyl]-carbamic acid tert-butyl ester

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Technology Process of [(S)-5-[(S)-3-tert-Butoxy-2-(11-imidazol-1-yl-undecanoylamino)-propionylamino]-5-(2-cyclohexyl-ethylcarbamoyl)-pentyl]-carbamic acid tert-butyl ester

There total 8 articles about [(S)-5-[(S)-3-tert-Butoxy-2-(11-imidazol-1-yl-undecanoylamino)-propionylamino]-5-(2-cyclohexyl-ethylcarbamoyl)-pentyl]-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68887-71-8
t-butyl 11-(1-imidazolyl)undecanoic acid

: 164931-18-4
Ser(O-t-Bu)-Lys(BOC)-2-cyclohexylethylamide

: 1026800-59-8
[(S)-5-[(S)-3-tert-Butoxy-2-(11-imidazol-1-yl-undecanoylamino)-propionylamino]-5-(2-cyclohexyl-ethylcarbamoyl)-pentyl]-carbamic acid tert-butyl ester

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1021/jm00011a001

Reference yield:

: 2-cyclohexylethanaminium acetate

: C₃₂H₅₇N₅O₇

: 1026800-59-8
[(S)-5-[(S)-3-tert-Butoxy-2-(11-imidazol-1-yl-undecanoylamino)-propionylamino]-5-(2-cyclohexyl-ethylcarbamoyl)-pentyl]-carbamic acid tert-butyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1039/c4ob01669f

Reference yield:

: 63632-65-5
11-iodo-undecanoic acid

: 1026800-59-8
[(S)-5-[(S)-3-tert-Butoxy-2-(11-imidazol-1-yl-undecanoylamino)-propionylamino]-5-(2-cyclohexyl-ethylcarbamoyl)-pentyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 18-crown-6 / dimethylformamide

2: DCC, HOBt / CH₂Cl₂; dimethylformamide / 0 - 20 °C

With 18-crown-6 ether; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00011a001