tert-butyl-(2-(4-((2,2,2-trifluoroacetamido)methyl)benzamido)phenyl)carbamate

Base Information

Chemical Name:tert-butyl-(2-(4-((2,2,2-trifluoroacetamido)methyl)benzamido)phenyl)carbamate
CAS No.:209784-84-9
Molecular Formula:C₂₁H₂₂F₃N₃O₄
Molecular Weight:437.419
Hs Code.:

Synonyms:tert-butyl-(2-(4-((2,2,2-trifluoroacetamido)methyl)benzamido)phenyl)carbamate

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Chemical Property of tert-butyl-(2-(4-((2,2,2-trifluoroacetamido)methyl)benzamido)phenyl)carbamate

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Technology Process of tert-butyl-(2-(4-((2,2,2-trifluoroacetamido)methyl)benzamido)phenyl)carbamate

There total 5 articles about tert-butyl-(2-(4-((2,2,2-trifluoroacetamido)methyl)benzamido)phenyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 24424-99-5
di-tert-butyl dicarbonate

: N-(2-aminophenyl)-4-((2,2,2-trifluoroacetamido)methyl)benzamide hydrochloride

: 209784-84-9
tert-butyl-(2-(4-((2,2,2-trifluoroacetamido)methyl)benzamido)phenyl)carbamate

Guidance literature:: With triethylamine; In dichloromethane; at 25 ℃; for 12h;
DOI:10.2174/1573406411666150714111045

Reference yield:

: C₁₀H₇ClF₃NO₂

: 146651-75-4
tert–butyl (2–aminophenyl)carbamate

: 209784-84-9
tert-butyl-(2-(4-((2,2,2-trifluoroacetamido)methyl)benzamido)phenyl)carbamate

Guidance literature:: at 20 ℃; for 20h;
DOI:10.1021/jm400634n

Reference yield:

: 130029-61-7
4-[[(2,2,2-trifluoroacetyl)amino]methyl]benzoic acid

: 209784-84-9
tert-butyl-(2-(4-((2,2,2-trifluoroacetamido)methyl)benzamido)phenyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide

2: 20 h / 20 °C

With oxalyl dichloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm400634n