2,3-dihydro-2,2'-bisindole

Base Information

• Chemical Name: 2,3-dihydro-2,2'-bisindole
• CAS No.: 38505-89-4
• Molecular Formula: C₁₆H₁₄N₂
• Molecular Weight: 234.301
• Mol file: 38505-89-4.mol

Synonyms:2,3-dihydro-2,2'-bisindole

Chemical Property of 2,3-dihydro-2,2'-bisindole

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

2-(Indolin-2-yl)-1H-indole 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-dihydro-2,2'-bisindole

There total 6 articles about 2,3-dihydro-2,2'-bisindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

1-acetyl-2,3-dihydro-2,2'-bisindole (172950-81-1) → 2,3-dihydro-2,2'-bisindole (38505-89-4)

Guidance literature:

With methanol; sodium methylate;

DOI:10.3987/COM-95-7192

Reference yield: 86.0%

1-acetyl-2,3-dihydro-2,2'-bisindole (172950-81-1) → 2,2'-biindole (40899-99-8) + 2,3-dihydro-2,2'-bisindole (38505-89-4)

Guidance literature:

With methanol; sodium; for 0.5h; Heating;

DOI:10.3987/COM-95-S4

Reference yield: 34.0%

1H,1'H-2,2'--bisindol--3--yl acetate (69423-26-3) → 2,3-dihydro-2,2'-bisindole (38505-89-4)

Guidance literature:

With acetic acid; zinc; Ambient temperature;

DOI:10.3987/COM-95-7192

upstream raw materials:

1-acetyl-2,3-dihydro-2,2'-bisindole

1H,1'H-2,2'--bisindol--3--yl acetate

1H,1H'-2,2'-Biindolylidene-3,3'-dione

indole

Downstream raw materials:

1-benzyl-2,3-dihydro-1H,1'H-[2,2']biindolyl

1-benzyl-2-(indol-2'-yl)indole