[3-(benzyl-tert-butoxycarbonyl-amino)-propyl]-(5-hydroxy-pentyl)-carbamic acid tert-butyl ester

Base Information

Chemical Name:[3-(benzyl-tert-butoxycarbonyl-amino)-propyl]-(5-hydroxy-pentyl)-carbamic acid tert-butyl ester
CAS No.:213772-93-1
Molecular Formula:C₂₅H₄₂N₂O₅
Molecular Weight:450.619
Hs Code.:

[3-(benzyl-<i>tert</i>-butoxycarbonyl-amino)-propyl]-(5-hydroxy-pentyl)-carbamic acid <i>tert</i>-butyl ester

Synonyms:[3-(benzyl-tert-butoxycarbonyl-amino)-propyl]-(5-hydroxy-pentyl)-carbamic acid tert-butyl ester

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Chemical Property of [3-(benzyl-tert-butoxycarbonyl-amino)-propyl]-(5-hydroxy-pentyl)-carbamic acid tert-butyl ester

Chemical Property:

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Technology Process of [3-(benzyl-tert-butoxycarbonyl-amino)-propyl]-(5-hydroxy-pentyl)-carbamic acid tert-butyl ester

There total 6 articles about [3-(benzyl-tert-butoxycarbonyl-amino)-propyl]-(5-hydroxy-pentyl)-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5433-11-4
N-Benzyliden-3-hydroxy-1-propanamin

: 213772-93-1
[3-(benzyl-tert-butoxycarbonyl-amino)-propyl]-(5-hydroxy-pentyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: NaBH₄ / ethanol / 2 h / 0 °C

2: CH₂Cl₂ / 3 h / 0 °C

3: 50 percent / Et₃N / diethyl ether / 3 h / 20 °C

4: K₂CO₃ / acetonitrile / 120 h / 20 °C

5: CH₂Cl₂ / 2 h / 0 °C

With sodium tetrahydroborate; potassium carbonate; triethylamine; In diethyl ether; ethanol; dichloromethane; acetonitrile; 1: Reduction / 2: Substitution / 3: Tosylation / 4: Substitution / 5: Substitution;
DOI:10.1016/S0968-0896(00)00055-9

Reference yield:

: 100-52-7
benzaldehyde

: 213772-93-1
[3-(benzyl-tert-butoxycarbonyl-amino)-propyl]-(5-hydroxy-pentyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: Na₂SO₄ / CH₂Cl₂ / 20 °C

2: NaBH₄ / ethanol / 2 h / 0 °C

3: CH₂Cl₂ / 3 h / 0 °C

4: 50 percent / Et₃N / diethyl ether / 3 h / 20 °C

5: K₂CO₃ / acetonitrile / 120 h / 20 °C

6: CH₂Cl₂ / 2 h / 0 °C

With sodium tetrahydroborate; potassium carbonate; sodium sulfate; triethylamine; In diethyl ether; ethanol; dichloromethane; acetonitrile; 1: Condensation / 2: Reduction / 3: Substitution / 4: Tosylation / 5: Substitution / 6: Substitution;
DOI:10.1016/S0968-0896(00)00055-9

Reference yield:

: 98014-76-7
3-[N-benzyl-N-(tert-butoxycarbonyl)amino]propan-1-ol

: 213772-93-1
[3-(benzyl-tert-butoxycarbonyl-amino)-propyl]-(5-hydroxy-pentyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / Et₃N / diethyl ether / 3 h / 20 °C

2: K₂CO₃ / acetonitrile / 120 h / 20 °C

3: CH₂Cl₂ / 2 h / 0 °C

With potassium carbonate; triethylamine; In diethyl ether; dichloromethane; acetonitrile; 1: Tosylation / 2: Substitution / 3: Substitution;
DOI:10.1016/S0968-0896(00)00055-9