C₆H₁₅N*C₈H₈BrNS₂

Base Information

• Chemical Name: C₆H₁₅N*C₈H₈BrNS₂
• CAS No.: 58655-25-7
• Molecular Formula: C₆H₁₅N*C₈H₈BrNS₂
• Molecular Weight: 363.386
• Mol file: 58655-25-7.mol

Synonyms:C₆H₁₅N*C₈H₈BrNS₂

Chemical Property of C₆H₁₅N*C₈H₈BrNS₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of C₆H₁₅N*C₈H₈BrNS₂

There total 1 articles about C₆H₁₅N*C₈H₈BrNS₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + 2-bromo-p-toluidine (583-68-6) + triethylamine (121-44-8) → C6H15N*C8H8BrNS2 (58655-25-7)

Guidance literature:

In tetrahydrofuran; at 20 ℃;

DOI:10.1021/ol9017535

Reference yield: 76.0%

4-tolyl iodide (624-31-7) + C6H15N*C8H8BrNS2 (58655-25-7) → 6-methyl-2-(p-tolylthio)-1,3-benzothiazole (1189350-87-5)

Guidance literature:

With copper(l) iodide; potassium carbonate; rac-diaminocyclohexane; In dimethyl sulfoxide; at 90 ℃; for 8h;

DOI:10.1021/ol9017535

Reference yield: 70.0%

C6H15N*C8H8BrNS2 (58655-25-7) → (2-bromo-4-methylphenyl)isothiocyanate (19241-39-5)

Guidance literature:

With ethyl triphenylphosphonium tribromide; triethylamine; In acetonitrile; Cooling with ice;

DOI:10.1080/00397910903531912

upstream raw materials:

carbon disulfide

2-bromo-p-toluidine

triethylamine

Downstream raw materials:

6-methyl-2-(p-tolylthio)-1,3-benzothiazole

(2-bromo-4-methylphenyl)isothiocyanate

2-bromo-4-methylphenylcyanamide

2-Bromo-4-methylphenylthiourea