2-(4-methoxyphenyl)-5-[4-(3,7-di-chloro-6-decyloxybenzo[b]thiophen-2-yl)phenyl]-1,3,4-oxadiazole

Base Information

Chemical Name:2-(4-methoxyphenyl)-5-[4-(3,7-di-chloro-6-decyloxybenzo[b]thiophen-2-yl)phenyl]-1,3,4-oxadiazole
CAS No.:1343465-16-6
Molecular Formula:C₃₃H₃₄Cl₂N₂O₃S
Molecular Weight:609.617
Hs Code.:

Synonyms:2-(4-methoxyphenyl)-5-[4-(3,7-di-chloro-6-decyloxybenzo[b]thiophen-2-yl)phenyl]-1,3,4-oxadiazole

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Chemical Property of 2-(4-methoxyphenyl)-5-[4-(3,7-di-chloro-6-decyloxybenzo[b]thiophen-2-yl)phenyl]-1,3,4-oxadiazole

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Technology Process of 2-(4-methoxyphenyl)-5-[4-(3,7-di-chloro-6-decyloxybenzo[b]thiophen-2-yl)phenyl]-1,3,4-oxadiazole

There total 3 articles about 2-(4-methoxyphenyl)-5-[4-(3,7-di-chloro-6-decyloxybenzo[b]thiophen-2-yl)phenyl]-1,3,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1343465-05-3
C₃₃H₄₀N₂O₄

: 1343465-11-1
2-(4-methoxyphenyl)-5-[4-(3-chloro-6-decyloxybenzo[b]thiophen-2-yl)phenyl]-1,3,4-oxadiazole

: 1343465-16-6
2-(4-methoxyphenyl)-5-[4-(3,7-di-chloro-6-decyloxybenzo[b]thiophen-2-yl)phenyl]-1,3,4-oxadiazole

Guidance literature:: With thionyl chloride; for 12h; Reflux; Inert atmosphere;
DOI:10.1016/j.tet.2011.09.060

Reference yield:

: 100-09-4
4-methoxybenzoic acid

: 1343465-11-1
2-(4-methoxyphenyl)-5-[4-(3-chloro-6-decyloxybenzo[b]thiophen-2-yl)phenyl]-1,3,4-oxadiazole

: 1343465-16-6
2-(4-methoxyphenyl)-5-[4-(3,7-di-chloro-6-decyloxybenzo[b]thiophen-2-yl)phenyl]-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 8 h / Reflux

2: pyridine / 2 h / 90 °C

3: thionyl chloride / 12 h / Reflux; Inert atmosphere

With pyridine; thionyl chloride;
DOI:10.1016/j.tet.2011.09.060

Reference yield:

: 1343465-00-8
C₂₅H₃₄N₂O₂

: 100-07-2
4-methoxy-benzoyl chloride

: 1343465-11-1
2-(4-methoxyphenyl)-5-[4-(3-chloro-6-decyloxybenzo[b]thiophen-2-yl)phenyl]-1,3,4-oxadiazole

: 1343465-16-6
2-(4-methoxyphenyl)-5-[4-(3,7-di-chloro-6-decyloxybenzo[b]thiophen-2-yl)phenyl]-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 2 h / 90 °C

2: thionyl chloride / 12 h / Reflux; Inert atmosphere

With pyridine; thionyl chloride;
DOI:10.1016/j.tet.2011.09.060