2',3'-DIFLUOROPROPIOPHENONE

Base Information

• Chemical Name: 2',3'-DIFLUOROPROPIOPHENONE
• CAS No.: 101712-19-0
• Molecular Formula: C₉H₈F₂O
• Molecular Weight: 170.159
• Hs Code.: 2914700090
• Mol file: 101712-19-0.mol

Synonyms:2,3-Difluoropropiophenone97%;2,3-DIFLUOROPROPIOPHENON;1-(2,3-difluorophenyl)propan-1-one;2,3-difluoro-1-phenylpropan-1-one

Chemical Property of 2',3'-DIFLUOROPROPIOPHENONE

Chemical Property:

• Boiling Point: 213.1 °C at 760 mmHg
• Flash Point: 79.8 °C
• PSA: 17.07000
• Density: 1.166 g/cm³
• LogP: 2.55750

Purity/Quality:

98%min ^*data from raw suppliers

2'',3''-Difluoropropiophenone ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2',3'-DIFLUOROPROPIOPHENONE

There total 2 articles about 2',3'-DIFLUOROPROPIOPHENONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(2,3-Difluorphenyl)-2-nitropropen (18355-83-4) → 1-(2,3-Difluoro-phenyl)-propan-2-one (101712-19-0)

Guidance literature:

With hydrogenchloride; iron(III) chloride; iron; In water;

DOI:10.1021/jm00156a009

Reference yield:

2,3-difluorobenzaldehyde (2646-91-5) → 1-(2,3-Difluoro-phenyl)-propan-2-one (101712-19-0)

Guidance literature:

Multi-step reaction with 2 steps

1: ammonium acetate

2: iron, ferric chloride hexahydrate, hydrochloric acid / H₂O

With ammonium acetate; hydrogenchloride; iron(III) chloride; iron; In water;

DOI:10.1021/jm00156a009

upstream raw materials:

1-(2,3-Difluorphenyl)-2-nitropropen

2,3-difluorobenzaldehyde

Refernces