benzhydryl 2α-(chloromethyl)-2β-methyl-6-diazopenam-3α-carboxylate 1β-oxide

Base Information

Chemical Name:benzhydryl 2α-(chloromethyl)-2β-methyl-6-diazopenam-3α-carboxylate 1β-oxide
CAS No.:115095-90-4
Molecular Formula:C₂₁H₁₈ClN₃O₄S
Molecular Weight:443.911
Hs Code.:

Synonyms:benzhydryl 2α-(chloromethyl)-2β-methyl-6-diazopenam-3α-carboxylate 1β-oxide

Suppliers and Price of benzhydryl 2α-(chloromethyl)-2β-methyl-6-diazopenam-3α-carboxylate 1β-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzhydryl 2α-(chloromethyl)-2β-methyl-6-diazopenam-3α-carboxylate 1β-oxide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzhydryl 2α-(chloromethyl)-2β-methyl-6-diazopenam-3α-carboxylate 1β-oxide

There total 5 articles about benzhydryl 2α-(chloromethyl)-2β-methyl-6-diazopenam-3α-carboxylate 1β-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115095-89-1
C₂₉H₂₆ClN₃O₆S

: 115095-90-4
benzhydryl 2α-(chloromethyl)-2β-methyl-6-diazopenam-3α-carboxylate 1β-oxide

Guidance literature:: With pyridine; In dichloromethane; for 3h; Yield given; Heating;
DOI:10.1021/jo00251a025

Reference yield:

: 64258-68-0
C₂₉H₂₆ClN₃O₅S

: 115095-90-4
benzhydryl 2α-(chloromethyl)-2β-methyl-6-diazopenam-3α-carboxylate 1β-oxide

Guidance literature:: Multi-step reaction with 5 steps

1: m-chloroperbenzoic acid / CH₂Cl₂ / 0.67 h / Ambient temperature

2: glacial acetic acid, Zn / CH₂Cl₂ / 1 h

3: 50 percent / toluene / 0.5 h / Heating

4: CH₃COONa, N₂O₄ / CH₂Cl₂ / 1 h

5: pyridine / CH₂Cl₂ / 3 h / Heating

With pyridine; sodium acetate; dinitrogen tetraoxide; acetic acid; 3-chloro-benzenecarboperoxoic acid; zinc; In dichloromethane; toluene;
DOI:10.1021/jo00251a025

Reference yield:

: 115095-88-0
benzhydryl 2α-(chloromethyl)-2β-methyl-6β-(phenylacetamido)penam-3α-carboxylate 1β-oxide

: 115095-90-4
benzhydryl 2α-(chloromethyl)-2β-methyl-6-diazopenam-3α-carboxylate 1β-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: CH₃COONa, N₂O₄ / CH₂Cl₂ / 1 h

2: pyridine / CH₂Cl₂ / 3 h / Heating

With pyridine; sodium acetate; dinitrogen tetraoxide; In dichloromethane;
DOI:10.1021/jo00251a025