[Rh((CHCHC₂H₄)2)(OAs(C₆H₅)3)(P(C₆H₅)3)]⁽¹⁺⁾*ClO₄^(1-)=[Rh((CHCHC₂H₄)2)(OAs(C₆H₅)3)(P(C₆H₅)3)]ClO₄

Base Information

• Chemical Name: [Rh((CHCHC₂H₄)2)(OAs(C₆H₅)3)(P(C₆H₅)3)]⁽¹⁺⁾*ClO₄^(1-)=[Rh((CHCHC₂H₄)2)(OAs(C₆H₅)3)(P(C₆H₅)3)]ClO₄
• CAS No.: 84191-01-5
• Molecular Formula: C₄₄H₄₂AsOPRh*ClO₄
• Molecular Weight: 895.068

Synonyms:[Rh((CHCHC₂H₄)2)(OAs(C₆H₅)3)(P(C₆H₅)3)]⁽¹⁺⁾*ClO₄^(1-)=[Rh((CHCHC₂H₄)2)(OAs(C₆H₅)3)(P(C₆H₅)3)]ClO₄

Chemical Property of [Rh((CHCHC₂H₄)2)(OAs(C₆H₅)3)(P(C₆H₅)3)]⁽¹⁺⁾*ClO₄^(1-)=[Rh((CHCHC₂H₄)2)(OAs(C₆H₅)3)(P(C₆H₅)3)]ClO₄

Chemical Property:

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Technology Process of [Rh((CHCHC₂H₄)2)(OAs(C₆H₅)3)(P(C₆H₅)3)]⁽¹⁺⁾*ClO₄^(1-)=[Rh((CHCHC₂H₄)2)(OAs(C₆H₅)3)(P(C₆H₅)3)]ClO₄

There total 4 articles about [Rh((CHCHC₂H₄)2)(OAs(C₆H₅)3)(P(C₆H₅)3)]⁽¹⁺⁾*ClO₄^(1-)=[Rh((CHCHC₂H₄)2)(OAs(C₆H₅)3)(P(C₆H₅)3)]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

[Rh((CHCHC2H4)2)(OAs(C6H5)3)2](1+)*ClO4(1-)=[Rh((CHCHC2H4)2)(OAs(C6H5)3)2]ClO4 (84190-91-0) → [Rh((CHCHC2H4)2)(OAs(C6H5)3)(P(C6H5)3)](1+)*ClO4(1-)=[Rh((CHCHC2H4)2)(OAs(C6H5)3)(P(C6H5)3)]ClO4 (84191-01-5)

Guidance literature:

With PPh₃; In dichloromethane; ligand added to complex soln. in molar ratio 1/1 at room temp.; concd. (vac.), pptd. with ether, filtered off, washed with ether or hexane, air-dried; elem. anal.;

DOI:10.1016/S0022-328X(00)85856-8

Reference yield:

[Rh2(OAs(C6H5)3)2((CHCHC2H4)2)2](2+)*2ClO4(1-)=[Rh2(OAs(C6H5)3)2((CHCHC2H4)2)2](ClO4)2 → [Rh((CHCHC2H4)2)(OAs(C6H5)3)(P(C6H5)3)](1+)*ClO4(1-)=[Rh((CHCHC2H4)2)(OAs(C6H5)3)(P(C6H5)3)]ClO4 (84191-01-5)

Guidance literature:

With PPh₃; In not given;

DOI:10.1016/S0022-328X(00)85856-8

Reference yield:

di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium (12092-47-6) → [Rh((CHCHC2H4)2)(OAs(C6H5)3)(P(C6H5)3)](1+)*ClO4(1-)=[Rh((CHCHC2H4)2)(OAs(C6H5)3)(P(C6H5)3)]ClO4 (84191-01-5)

Guidance literature:

Multi-step reaction with 2 steps

1: acetone

2: PPh₃ / dichloromethane

With PPh₃; In dichloromethane; acetone;

DOI:10.1016/S0022-328X(00)85856-8

upstream raw materials:

[Rh((CHCHC₂H₄)2)(OAs(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh((CHCHC₂H₄)2)(OAs(C₆H₅)3)2]ClO₄

[Rh(CO)2(OAs(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)2(OAs(C₆H₅)3)2]ClO₄

di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

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