[¹³C, D_3]-p-nitromethoxybenzene

Base Information

• Chemical Name: [¹³C, D_3]-p-nitromethoxybenzene
• CAS No.: 1404479-74-8
• Molecular Formula: C₇H₇NO₃
• Molecular Weight: 157.103

Synonyms:[¹³C, D_3]-p-nitromethoxybenzene

Chemical Property of [¹³C, D_3]-p-nitromethoxybenzene

Chemical Property:

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Technology Process of [¹³C, D_3]-p-nitromethoxybenzene

There total 1 articles about [¹³C, D_3]-p-nitromethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + [13C2H3] methyl iodide (20710-47-8,207507-22-0) → [13C, D3]-p-nitromethoxybenzene (1404479-74-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 14h;

DOI:10.1002/anie.201202885

Reference yield: 27.0%

[13C, D3]-p-nitromethoxybenzene (1404479-74-8) → [13C, D3]-p-anisidine (1404479-73-7)

Guidance literature:

With 10% Pd/C; hydrogen; In ethanol; at 20 ℃; for 41h;

DOI:10.1002/anie.201202885

upstream raw materials:

4-nitro-phenol

[13C₂H₃] methyl iodide

Downstream raw materials:

[¹³C, D₃]-p-anisidine

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