C₂₃H₃₂O₃Si

Base Information

Chemical Name:C₂₃H₃₂O₃Si
CAS No.:1417795-86-8
Molecular Formula:C₂₃H₃₂O₃Si
Molecular Weight:384.591
Hs Code.:

C<sub>23</sub>H<sub>32</sub>O<sub>3</sub>Si

Synonyms:C₂₃H₃₂O₃Si

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Chemical Property of C₂₃H₃₂O₃Si

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Technology Process of C₂₃H₃₂O₃Si

There total 15 articles about C₂₃H₃₂O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: (4S)-5-(tert-butyldiphenylsilyloxy)-2,4-dimethylpentan-1-ol

: 1417795-86-8
C₂₃H₃₂O₃Si

: 157837-64-4
(2R,4S)-5-{[tert-butyl(diphenyl)silyl]oxy}-2,4-dimethylpentan-1-ol

Guidance literature:: With Gluconobacter oxydans; In 2,2,4-trimethylpentane; at 20 ℃; for 2h; Time; Enzymatic reaction;
DOI:10.1016/j.tet.2012.11.051

Reference yield: 35.0%

: (4S)-5-(tert-butyldiphenylsilyloxy)-2,4-dimethylpentan-1-ol

: 1417795-86-8
C₂₃H₃₂O₃Si

: 157837-64-4
(2R,4S)-5-{[tert-butyl(diphenyl)silyl]oxy}-2,4-dimethylpentan-1-ol

: (R)-4-benzyl-3-((4S,6S)-7-((tert-butyldiphenylsilyl)oxy)-4,6-dimethylhept-2-enoyl)oxazolidin-2-one

Guidance literature:: With Glucose oxidase from Aspergillus niger; In aq. phosphate buffer; dichloromethane; at 25 ℃; for 1h; pH=8; Inert atmosphere; Enzymatic reaction;
DOI:10.1016/j.tetasy.2015.07.001

Reference yield:

: 91751-24-5,92817-88-4,123284-89-9,112897-04-8
(R)-3-[(tert-butyldiphenylsilyl)oxy]-2-methylpropanal

: 1417795-86-8
C₂₃H₃₂O₃Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: dichloromethane / 24.5 h / 0 - 20 °C / Inert atmosphere

2.1: nickel dichloride / methanol / 0.5 h / 0 °C

2.2: 0 - 20 °C

3.1: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 °C

4.1: Gluconobacter oxydans / 2,2,4-trimethylpentane / 2 h / 20 °C / Enzymatic reaction

With lithium aluminium tetrahydride; nickel dichloride; In methanol; 2,2,4-trimethylpentane; diethyl ether; dichloromethane; 1.1: |Wittig Olefination;
DOI:10.1016/j.tet.2012.11.051