N¹-(3-(amino(hydroxyimino)methyl)benzoyl)-N²-(4-tert-butylbenzoyl)-1,2-benzenediamine

Base Information

• Chemical Name: N¹-(3-(amino(hydroxyimino)methyl)benzoyl)-N²-(4-tert-butylbenzoyl)-1,2-benzenediamine
• CAS No.: 219519-01-4
• Molecular Formula: C₂₅H₂₆N₄O₃
• Molecular Weight: 430.506

Synonyms:N¹-(3-(amino(hydroxyimino)methyl)benzoyl)-N²-(4-tert-butylbenzoyl)-1,2-benzenediamine

Chemical Property of N¹-(3-(amino(hydroxyimino)methyl)benzoyl)-N²-(4-tert-butylbenzoyl)-1,2-benzenediamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N¹-(3-(amino(hydroxyimino)methyl)benzoyl)-N²-(4-tert-butylbenzoyl)-1,2-benzenediamine

There total 6 articles about N¹-(3-(amino(hydroxyimino)methyl)benzoyl)-N²-(4-tert-butylbenzoyl)-1,2-benzenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

N1-(3-cyanobenzoyl)-N2-(4-t-butylbenzoyl)-1,2-benzenediamine (219492-02-1) → N1-(3-(amino(hydroxyimino)methyl)benzoyl)-N2-(4-tert-butylbenzoyl)-1,2-benzenediamine (219519-01-4)

Guidance literature:

With hydroxylamine hydrochloride; N-ethyl-N,N-diisopropylamine; In ethanol; Heating;

DOI:10.1021/jm9903287

Reference yield: 55.0%

N1-(3-cyanobenzoyl)-N2-(4-t-butylbenzoyl)-1,2-benzenediamine (219492-02-1) → N1-[3-(amino(hydroxyimino)methyl)benzoyl]-N2-(4-t-butylbenzoyl)-1,2-benzenediamine (219519-01-4)

Guidance literature:

Reference yield:

2-nitro-aniline (88-74-4) → N1-(3-(amino(hydroxyimino)methyl)benzoyl)-N2-(4-tert-butylbenzoyl)-1,2-benzenediamine (219519-01-4)

Guidance literature:

Multi-step reaction with 4 steps

1: 100 percent / pyridine

2: 79 percent / H₂ / Pd/C / ethyl acetate

3: 87 percent / triethylamine / CH₂Cl₂ / 20 °C

4: 55 percent / NH₂OH*HCl; iPr₂NEt / ethanol / Heating

With pyridine; hydroxylamine hydrochloride; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; dichloromethane; ethyl acetate; 1: Acylation / 2: Reduction / 3: Acylation / 4: Addition;

DOI:10.1021/jm9903287

upstream raw materials:

N¹-(3-cyanobenzoyl)-N²-(4-t-butylbenzoyl)-1,2-benzenediamine

2-nitro-aniline

p-tert-butyl benzoyl chloride

N-(2-aminophenyl)-4-(1,1-dimethylethyl)-benzamide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 219519-01-4 N¹-(3-(amino(hydroxyimino)methyl)benzoyl)-N²-(4-tert-butylbenzoyl)-1,2-benzenediamine

Send

Send

Metric Ton KG G Pound L ML

Send

Send