Technology Process of C34H43NO7S
There total 5 articles about C34H43NO7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at 20 ℃;
for 2h;
Cooling with ice;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: toluene / Reflux
2.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 2068.65 Torr / Inert atmosphere
2.2: 2 h / 20 °C / Cooling with ice
3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C / Inert atmosphere; Cooling with ice
3.2: 20 °C / Cooling with ice
4.1: triethylamine / dichloromethane / 2 h / 20 °C / Cooling with ice; Inert atmosphere
With
hydrogen; sodium hydride; triethylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; dichloromethane; toluene; mineral oil;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 90 °C
2.1: toluene / Reflux
3.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 2068.65 Torr / Inert atmosphere
3.2: 2 h / 20 °C / Cooling with ice
4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C / Inert atmosphere; Cooling with ice
4.2: 20 °C / Cooling with ice
5.1: triethylamine / dichloromethane / 2 h / 20 °C / Cooling with ice; Inert atmosphere
With
hydrogen; sodium hydride; sodium hydrogencarbonate; triethylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil;