O⁷-benzyl glaziovianin A

Base Information

Chemical Name:O⁷-benzyl glaziovianin A
CAS No.:1252801-65-2
Molecular Formula:C₂₆H₂₂O₈
Molecular Weight:462.456
Hs Code.:

Synonyms:O⁷-benzyl glaziovianin A

Suppliers and Price of O⁷-benzyl glaziovianin A

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O⁷-benzyl glaziovianin A

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of O⁷-benzyl glaziovianin A

There total 8 articles about O⁷-benzyl glaziovianin A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1252801-64-1
O⁷-demethyl glaziovianin A

: 100-39-0
benzyl bromide

: 1252801-65-2
O⁷-benzyl glaziovianin A

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃;
DOI:10.1016/j.bmcl.2010.07.111

Reference yield: 61.0%

: 2-(4,7-dimethoxybenzo[d][1,3]dioxol-5-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 7-(benzyloxy)-3-iodo-6-methoxy-4H-chromen-4-one

: 1252801-65-2
O⁷-benzyl glaziovianin A

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium carbonate; In 1,4-dioxane; water; at 20 ℃; for 15h; Inert atmosphere;
DOI:10.1021/acsmedchemlett.9b00526

Reference yield:

: 7298-21-7
1-(2,4-dihydroxy-5-methoxyphenyl)ethan-1-one

: 1252801-65-2
O⁷-benzyl glaziovianin A

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridinium p-toluenesulfonate / dichloromethane

2.1: 12 h / 90 °C

3.1: pyridine; iodine / chloroform / 12 h / 0 - 20 °C / Darkness

4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium carbonate / 1,4-dioxane; water / 24 h / 20 °C / Inert atmosphere

4.2: SiliaBond / 0.5 h / 20 °C

5.1: toluene-4-sulfonic acid / chloroform; methanol / 3 h / 20 °C

6.1: potassium carbonate / acetonitrile / 5 h / 20 °C

With pyridine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; iodine; pyridinium p-toluenesulfonate; sodium carbonate; potassium carbonate; toluene-4-sulfonic acid; In 1,4-dioxane; methanol; dichloromethane; chloroform; water; acetonitrile;
DOI:10.1016/j.bmc.2012.08.005