4-nitrophenyl methylphosphonothiochloridate

Base Information

• Chemical Name: 4-nitrophenyl methylphosphonothiochloridate
• CAS No.: 27976-51-8
• Molecular Formula: C₇H₇ClNO₃PS
• Molecular Weight: 251.63

Synonyms:4-nitrophenyl methylphosphonothiochloridate

Chemical Property of 4-nitrophenyl methylphosphonothiochloridate

Chemical Property:

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Technology Process of 4-nitrophenyl methylphosphonothiochloridate

There total 3 articles about 4-nitrophenyl methylphosphonothiochloridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + methylphosphonothioic dichloride (676-98-2) → 4-nitrophenyl methylphosphonothiochloridate (27976-51-8)

Guidance literature:

With TEA; In toluene; for 8h; Heating;

DOI:10.1016/S0040-4039(02)00735-9

Reference yield:

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + 2,4-dimethyl-1,3,2,4-dithiadiphosphetane 2,4-disulfide (1121-81-9) → 4-nitrophenyl methylphosphonothiochloridate (27976-51-8)

Guidance literature:

Multistep reaction; (i), (ii) SO₂Cl₂;

DOI:10.1021/jo01058a018

Reference yield:

→ 4-nitrophenyl methylphosphonothiochloridate (27976-51-8)

Guidance literature:

MePSCl2, p-Nitrophenol;

DOI:10.1021/je60046a030

upstream raw materials:

4-nitro-phenol

2,4-dimethyl-1,3,2,4-dithiadiphosphetane 2,4-disulfide

methylphosphonothioic dichloride

Downstream raw materials:

C₁₅H₁₇N₂O₃PS

C₁₅H₁₇N₂O₃PS

methyl-phosphonothioic acid O-isopropyl ester O-(4-nitro-phenyl) ester

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