4-phenyl-NNO-azoxybenzonitrile

Base Information

• Chemical Name: 4-phenyl-NNO-azoxybenzonitrile
• CAS No.: 115976-70-0
• Molecular Formula: C₁₃H₉N₃O
• Molecular Weight: 223.234
• Mol file: 115976-70-0.mol

Synonyms:4-phenyl-NNO-azoxybenzonitrile

Chemical Property of 4-phenyl-NNO-azoxybenzonitrile

Chemical Property:

Purity/Quality:

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Technology Process of 4-phenyl-NNO-azoxybenzonitrile

There total 1 articles about 4-phenyl-NNO-azoxybenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

copper(I) cyanide (544-92-3) + 4-bromo-1-phenyl-NNO-azoxybenzene (16109-68-5,132872-19-6) → 4-phenyl-NNO-azoxybenzonitrile (115976-70-0)

Guidance literature:

In N,N-dimethyl-formamide; at 155 - 160 ℃; for 4h;

DOI:10.1039/P29880000147

Reference yield:

4-phenyl-NNO-azoxybenzonitrile (115976-70-0) → 4-phenyl-NNO-azoxybenzoic acid (105595-96-8)

Guidance literature:

With sodium hydroxide; dihydrogen peroxide; sodium hydroxide; In ethanol; at 45 - 50 ℃; for 2h;

DOI:10.1039/P29880000147

upstream raw materials:

copper(I) cyanide

4-bromo-1-phenyl-NNO-azoxybenzene

Downstream raw materials:

4-phenyl-NNO-azoxybenzoic acid