Technology Process of 7α-benzyloxymethyl-6β-indol-3'-yl-7β,9-dimethyl-5,6α,6aβ,7β,8,10aβ-hexahydroindeno<2,1-b>indole
There total 8 articles about 7α-benzyloxymethyl-6β-indol-3'-yl-7β,9-dimethyl-5,6α,6aβ,7β,8,10aβ-hexahydroindeno<2,1-b>indole which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
disodium hydrogenphosphate; sodium amalgam;
In
methanol; diethyl ether;
for 1h;
Ambient temperature;
DOI:10.1016/0223-5234(92)90100-F
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 75 percent / BF3*Et2O / tetrahydrofuran / 4 h / Ambient temperature
2: 85 percent / 5percent Na-Hg, Na2HPO4 / diethyl ether; methanol / 1 h / Ambient temperature
With
disodium hydrogenphosphate; sodium amalgam; boron trifluoride diethyl etherate;
In
tetrahydrofuran; methanol; diethyl ether;
DOI:10.1016/0223-5234(92)90100-F
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 87 percent / n-Bu4NHSO4, 50percent NaOH / benzene / 0.5 h / Ambient temperature
2: 75 percent / BF3*Et2O / tetrahydrofuran / 4 h / Ambient temperature
3: 85 percent / 5percent Na-Hg, Na2HPO4 / diethyl ether; methanol / 1 h / Ambient temperature
With
sodium hydroxide; disodium hydrogenphosphate; sodium amalgam; boron trifluoride diethyl etherate; tetra(n-butyl)ammonium hydrogensulfate;
In
tetrahydrofuran; methanol; diethyl ether; benzene;
DOI:10.1016/0223-5234(92)90100-F
