C₄₆H₃₈N₂O₈

Base Information

Chemical Name:C₄₆H₃₈N₂O₈
CAS No.:1610027-13-8
Molecular Formula:C₄₆H₃₈N₂O₈
Molecular Weight:746.816
Hs Code.:

C<sub>46</sub>H<sub>38</sub>N<sub>2</sub>O<sub>8</sub>

Synonyms:C₄₆H₃₈N₂O₈

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Chemical Property of C₄₆H₃₈N₂O₈

Chemical Property:

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Technology Process of C₄₆H₃₈N₂O₈

There total 10 articles about C₄₆H₃₈N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1610027-11-6
(2S,4aR,7aS,9S,11aR,14aS)-7a,14a-bis(benzyloxy)-2,9-dihydroxy-1,7a,8,9,11a,14a-hexahydropyrazino[1,2-a:4,5-a']diindole-6,13(2H,4aH)-dione

: 98-88-4
benzoyl chloride

: 1610027-13-8
C₄₆H₃₈N₂O₈

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol500990f

Reference yield:

: C₇H₇BrO₂

: 1610027-13-8
C₄₆H₃₈N₂O₈

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium tetrahydroborate / tetrahydrofuran; water / -78 - 0 °C

2.1: potassium carbonate; 18-crown-6 ether / water; 1,4-dioxane / 20 h / Reflux

3.1: camphor-10-sulfonic acid / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

3.2: 4 h / 0 °C

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 - -70 °C / Inert atmosphere

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 48 h / -70 - 0 °C / Inert atmosphere

6.1: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

7.1: potassium carbonate / tetrahydrofuran; methanol / 0.5 h / Inert atmosphere

8.1: triethylamine; dmap / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; dmap; sodium tetrahydroborate; oxalyl dichloride; 18-crown-6 ether; camphor-10-sulfonic acid; potassium carbonate; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; 4.1: |Swern Oxidation;
DOI:10.1021/ol500990f

Reference yield:

: 1610027-05-8
((1S,2R,4S)-2-bromo-7-oxabicyclo[2.2.1]hept-5-en-2-yl)methanol

: 1610027-13-8
C₄₆H₃₈N₂O₈

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate; 18-crown-6 ether / water; 1,4-dioxane / 20 h / Reflux

2.1: camphor-10-sulfonic acid / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

2.2: 4 h / 0 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 - -70 °C / Inert atmosphere

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 48 h / -70 - 0 °C / Inert atmosphere

5.1: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

6.1: potassium carbonate / tetrahydrofuran; methanol / 0.5 h / Inert atmosphere

7.1: triethylamine; dmap / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; dmap; oxalyl dichloride; 18-crown-6 ether; camphor-10-sulfonic acid; potassium carbonate; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; 3.1: |Swern Oxidation;
DOI:10.1021/ol500990f