3-(4-bromophenyl)-3-o-tolylpropanoic acid

Base Information

Chemical Name:3-(4-bromophenyl)-3-o-tolylpropanoic acid
CAS No.:1354808-43-7
Molecular Formula:C₁₆H₁₅BrO₂
Molecular Weight:319.198
Hs Code.:

Synonyms:3-(4-bromophenyl)-3-o-tolylpropanoic acid

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Chemical Property of 3-(4-bromophenyl)-3-o-tolylpropanoic acid

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Technology Process of 3-(4-bromophenyl)-3-o-tolylpropanoic acid

There total 5 articles about 3-(4-bromophenyl)-3-o-tolylpropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1354808-42-6
ethyl 3-(4-bromophenyl)-2-cyano-3-o-tolylpropanoate

: 1354808-43-7
3-(4-bromophenyl)-3-o-tolylpropanoic acid

Guidance literature:: With sulfuric acid; acetic acid; at 27 ℃; for 20.5h; Reflux;

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 1354808-43-7
3-(4-bromophenyl)-3-o-tolylpropanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: piperidine / toluene / 5 h / Reflux; Dean-Stark

2: toluene; tetrahydrofuran / 2.83 h / 0 - 85 °C

3: sulfuric acid; acetic acid / 20 h / 27 °C / Reflux

With piperidine; sulfuric acid; acetic acid; In tetrahydrofuran; toluene;

Reference yield:

: 42205-33-4
(E)-ethyl 3-(4-bromophenyl)-2-cyanoacrylate

: 1354808-43-7
3-(4-bromophenyl)-3-o-tolylpropanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: toluene; tetrahydrofuran / 2.83 h / 0 - 85 °C

2: sulfuric acid; acetic acid / 20 h / 27 °C / Reflux

With sulfuric acid; acetic acid; In tetrahydrofuran; toluene;