(E)-(4-fluoro-2-nitrophenyl)ethanal semicarbazone

Base Information

Chemical Name:(E)-(4-fluoro-2-nitrophenyl)ethanal semicarbazone
CAS No.:1065183-63-2
Molecular Formula:C₉H₉FN₄O₃
Molecular Weight:240.194
Hs Code.:

Synonyms:(E)-(4-fluoro-2-nitrophenyl)ethanal semicarbazone

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Chemical Property of (E)-(4-fluoro-2-nitrophenyl)ethanal semicarbazone

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Technology Process of (E)-(4-fluoro-2-nitrophenyl)ethanal semicarbazone

There total 2 articles about (E)-(4-fluoro-2-nitrophenyl)ethanal semicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (E)-1-(4-fluoro-2-nitrostyryl)pyrrolidine

: 563-41-7
semicarbazide hydrochloride

: 1065183-63-2
(E)-(4-fluoro-2-nitrophenyl)ethanal semicarbazone

Guidance literature:: In methanol; water; at 20 ℃; for 1h; Inert atmosphere;

Reference yield:

: 446-10-6
2-nitro-4-fluorotoluene

: 1065183-63-2
(E)-(4-fluoro-2-nitrophenyl)ethanal semicarbazone

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / Inert atmosphere; Reflux

2: methanol; water / 1 h / 20 °C / Inert atmosphere

In methanol; water; N,N-dimethyl-formamide;

Reference yield: 87.0%

: 1065183-63-2
(E)-(4-fluoro-2-nitrophenyl)ethanal semicarbazone

: 399-51-9
6-fluoro-1H-indole

Guidance literature:: With hydrogen; iron(II) acetate; 5% rhodium-on-charcoal; In tetrahydrofuran; toluene; at 20 ℃; for 48h; under 38002.6 Torr; Inert atmosphere;