3-methoxy-2-(4-tolylthio)phenyl isopropylcarbamate

Base Information

Chemical Name:3-methoxy-2-(4-tolylthio)phenyl isopropylcarbamate
CAS No.:1609120-01-5
Molecular Formula:C₁₈H₂₁NO₃S
Molecular Weight:331.436
Hs Code.:

Synonyms:3-methoxy-2-(4-tolylthio)phenyl isopropylcarbamate

Suppliers and Price of 3-methoxy-2-(4-tolylthio)phenyl isopropylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-methoxy-2-(4-tolylthio)phenyl isopropylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-methoxy-2-(4-tolylthio)phenyl isopropylcarbamate

There total 2 articles about 3-methoxy-2-(4-tolylthio)phenyl isopropylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 956219-13-9
3-methoxyphenyl isopropylcarbamate

: 2943-42-2
di(4-methyl)phenylthiosulfonate

: 1609120-01-5
3-methoxy-2-(4-tolylthio)phenyl isopropylcarbamate

Guidance literature:: 3-methoxyphenyl isopropylcarbamate; With tert-butyldimethylsilyl triflate; N,N,N,N,-tetramethylethylenediamine; In diethyl ether; at 0 - 20 ℃; for 0.583333h; Inert atmosphere;

With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 1h; Inert atmosphere;

di(4-methyl)phenylthiosulfonate; In diethyl ether; hexane; at -78 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1246/cl.130899

Reference yield:

: 150-19-6
O-methylresorcine

: 1609120-01-5
3-methoxy-2-(4-tolylthio)phenyl isopropylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere

2.1: tert-butyldimethylsilyl triflate; N,N,N,N,-tetramethylethylenediamine / diethyl ether / 0.58 h / 0 - 20 °C / Inert atmosphere

2.2: 1 h / -78 °C / Inert atmosphere

2.3: 12 h / -78 - 20 °C / Inert atmosphere

With tert-butyldimethylsilyl triflate; N,N,N,N,-tetramethylethylenediamine; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1246/cl.130899

Reference yield: 63.0%

: 1609120-01-5
3-methoxy-2-(4-tolylthio)phenyl isopropylcarbamate

: 1609120-02-6
3-methoxy-2-(4-tolylthio)phenol

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; diethylamine; In acetonitrile; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1246/cl.130899