[Mo(N((t)Bu)(C₆H₃-3,5-Me₂))3NC(O)Ph]O₃SCF₃

Base Information

Chemical Name:[Mo(N((t)Bu)(C₆H₃-3,5-Me₂))3NC(O)Ph]O₃SCF₃
CAS No.:819799-81-0
Molecular Formula:CF₃O₃S*C₄₃H₅₉MoN₄O
Molecular Weight:892.978
Hs Code.:

[Mo(N((t)Bu)(C<sub>6</sub>H<sub>3</sub>-3,5-Me<sub>2</sub>))3NC(O)Ph]O<sub>3</sub>SCF<sub>3</sub>

Synonyms:[Mo(N((t)Bu)(C₆H₃-3,5-Me₂))3NC(O)Ph]O₃SCF₃

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Chemical Property of [Mo(N((t)Bu)(C₆H₃-3,5-Me₂))3NC(O)Ph]O₃SCF₃

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Technology Process of [Mo(N((t)Bu)(C₆H₃-3,5-Me₂))3NC(O)Ph]O₃SCF₃

There total 2 articles about [Mo(N((t)Bu)(C₆H₃-3,5-Me₂))3NC(O)Ph]O₃SCF₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 256240-25-2
NMo(N[((t)Bu)(3,5-C₆H₃Me₂)])3

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 98-88-4
benzoyl chloride

: 819799-81-0
[Mo(N((t)Bu)(C₆H₃-3,5-Me₂))3NC(O)Ph]O₃SCF₃

Guidance literature:: treatment of molybdenum compd. with trimethylsilyl deriv.; treatment with 1.25 equiv. of benzoyl chloride in presence of 0.2 equiv. of pyridine;
DOI:10.1021/ja066090a

Reference yield: 72.0%

: 256240-25-2
NMo(N[((t)Bu)(3,5-C₆H₃Me₂)])3

: 36967-85-8
benzoyl triflate

: 819799-81-0
[Mo(N((t)Bu)(C₆H₃-3,5-Me₂))3NC(O)Ph]O₃SCF₃

Guidance literature:: In dichloromethane; under N2, triflate-compd. in CH2Cl2 was added to CH2Cl2 soln. of Mo-compd. at -35 °C, stirring at 25 °C for 1 h; soln. was concd., cold Et2O was added, ppt. was filtered off, washed with pentane, recrystn. from concd. THF layered with pentane, elem. anal.;
DOI:10.1016/j.poly.2004.08.010