phenyl β-D-galactopyranosyl-(1->3)-2-amino-2-deoxy-1-thio-β-D-glucopyranoside

Base Information

• Chemical Name: phenyl β-D-galactopyranosyl-(1->3)-2-amino-2-deoxy-1-thio-β-D-glucopyranoside
• CAS No.: 1174733-84-6
• Molecular Formula: C₁₈H₂₇NO₉S
• Molecular Weight: 433.48
• Mol file: 1174733-84-6.mol

Synonyms:phenyl β-D-galactopyranosyl-(1->3)-2-amino-2-deoxy-1-thio-β-D-glucopyranoside

Chemical Property of phenyl β-D-galactopyranosyl-(1->3)-2-amino-2-deoxy-1-thio-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenyl β-D-galactopyranosyl-(1->3)-2-amino-2-deoxy-1-thio-β-D-glucopyranoside

There total 1 articles about phenyl β-D-galactopyranosyl-(1->3)-2-amino-2-deoxy-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

α-galactosyl fluoride (2021-84-3) + phenyl 2-amino-2-deoxy-1-thio-β-D-glucopyranoside hydrochloride (1174733-83-5) → phenyl β-D-galactopyranosyl-(1->3)-2-amino-2-deoxy-1-thio-β-D-glucopyranoside (1174733-84-6)

Guidance literature:

α-galactosyl fluoride; phenyl 2-amino-2-deoxy-1-thio-β-D-glucopyranoside hydrochloride; With Thermus thermophilus glycosynthase E₃₃₈G; at 37 ℃; aq. phosphate buffer;

With ammonium hydroxide; In methanol; chloroform;

DOI:10.1016/j.tetasy.2009.05.007

Reference yield: 94.0%

phenyl β-D-galactopyranosyl-(1->3)-2-amino-2-deoxy-1-thio-β-D-glucopyranoside (1174733-84-6) + acetic anhydride (108-24-7) → phenyl β-D-galactopyranosyl-(1->3)-2-acetamido-2-deoxy-1-thio-β-D-glucopyranoside (1174733-85-7)

Guidance literature:

With sodium hydrogencarbonate; In methanol; at 20 ℃; for 0.75h;

DOI:10.1016/j.tetasy.2009.05.007

upstream raw materials:

α-galactosyl fluoride

phenyl 2-amino-2-deoxy-1-thio-β-D-glucopyranoside hydrochloride

Downstream raw materials:

phenyl β-D-galactopyranosyl-(1->3)-2-acetamido-2-deoxy-1-thio-β-D-glucopyranoside