5-O-Acetyl-1-N-benzyl-2',3,6'-tris-N-(benzyloxycarbonyl)-1-N,6-O-carbonylsisamin

Base Information

Chemical Name:5-O-Acetyl-1-N-benzyl-2',3,6'-tris-N-(benzyloxycarbonyl)-1-N,6-O-carbonylsisamin
CAS No.:97119-55-6
Molecular Formula:C₄₆H₄₈N₄O₁₂
Molecular Weight:848.907
Hs Code.:

Synonyms:5-O-Acetyl-1-N-benzyl-2',3,6'-tris-N-(benzyloxycarbonyl)-1-N,6-O-carbonylsisamin

Suppliers and Price of 5-O-Acetyl-1-N-benzyl-2',3,6'-tris-N-(benzyloxycarbonyl)-1-N,6-O-carbonylsisamin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-O-Acetyl-1-N-benzyl-2',3,6'-tris-N-(benzyloxycarbonyl)-1-N,6-O-carbonylsisamin

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-O-Acetyl-1-N-benzyl-2',3,6'-tris-N-(benzyloxycarbonyl)-1-N,6-O-carbonylsisamin

There total 2 articles about 5-O-Acetyl-1-N-benzyl-2',3,6'-tris-N-(benzyloxycarbonyl)-1-N,6-O-carbonylsisamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 108-24-7
acetic anhydride

: 97119-54-5
1-N-Benzyl-2',3,6'-tris-N-(benzyloxycarbonyl)-1-N,6-O-carbonylsisamin

: 97119-55-6
5-O-Acetyl-1-N-benzyl-2',3,6'-tris-N-(benzyloxycarbonyl)-1-N,6-O-carbonylsisamin

Guidance literature:: In pyridine; at 20 ℃; for 1h;
DOI:10.1002/jlac.198519850511

Reference yield:

: 100-39-0
benzyl bromide

: 97119-55-6
5-O-Acetyl-1-N-benzyl-2',3,6'-tris-N-(benzyloxycarbonyl)-1-N,6-O-carbonylsisamin

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaH / 1) DMF, 0 deg C, 2) toluene, from 0 deg C to room temp.; 1 h, room temp.

2: 93 percent / pyridine / 1 h / 20 °C

With sodium hydride; In pyridine;
DOI:10.1002/jlac.198519850511