3-methyl-5-nitro-1-phenyluracil

Base Information Edit

Chemical Name:3-methyl-5-nitro-1-phenyluracil
CAS No.:934802-64-9
Molecular Formula:C₁₁H₉N₃O₄
Molecular Weight:247.21
Hs Code.:
Mol file:934802-64-9.mol

Synonyms:3-methyl-5-nitro-1-phenyluracil

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-methyl-5-nitro-1-phenyluracil Edit

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Technology Process of 3-methyl-5-nitro-1-phenyluracil

There total 2 articles about 3-methyl-5-nitro-1-phenyluracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 903572-34-9
1-(2,4-dinitrophenyl)-3-methyl-5-nitrouracil

: 62-53-3
aniline

: 934802-64-9
3-methyl-5-nitro-1-phenyluracil

: 97-02-9
2,4-Dinitroanilin

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.tet.2007.01.040

Reference yield:

: 934802-62-7
1-(2,4-dinitrophenyl)-3-methyluracil

: 934802-64-9
3-methyl-5-nitro-1-phenyluracil

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / nitric acid / H₂SO₄ / 4 h / 20 °C

2: 56 percent / dimethylformamide / 20 °C

With nitric acid; In sulfuric acid; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.01.040