1-chloro-2-(4-methoxy-benzyl)-4-[2,3-O-(2,3-dimethoxy-buta-2,3-diyl)-β-D-glucopyranos-1-yl]-benzene

Base Information

Chemical Name:1-chloro-2-(4-methoxy-benzyl)-4-[2,3-O-(2,3-dimethoxy-buta-2,3-diyl)-β-D-glucopyranos-1-yl]-benzene
CAS No.:872980-39-7
Molecular Formula:C₂₆H₃₃ClO₈
Molecular Weight:508.996
Hs Code.:

Synonyms:1-chloro-2-(4-methoxy-benzyl)-4-[2,3-O-(2,3-dimethoxy-buta-2,3-diyl)-β-D-glucopyranos-1-yl]-benzene

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Chemical Property of 1-chloro-2-(4-methoxy-benzyl)-4-[2,3-O-(2,3-dimethoxy-buta-2,3-diyl)-β-D-glucopyranos-1-yl]-benzene

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Technology Process of 1-chloro-2-(4-methoxy-benzyl)-4-[2,3-O-(2,3-dimethoxy-buta-2,3-diyl)-β-D-glucopyranos-1-yl]-benzene

There total 2 articles about 1-chloro-2-(4-methoxy-benzyl)-4-[2,3-O-(2,3-dimethoxy-buta-2,3-diyl)-β-D-glucopyranos-1-yl]-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 333359-90-3
(2S,3R,4R,5S,6R)-2-(4-chloro-3-(4-methoxybenzyl)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol

: 431-03-8
dimethylglyoxal

: 149-73-5
trimethyl orthoformate

: 872980-39-7
1-chloro-2-(4-methoxy-benzyl)-4-[2,3-O-(2,3-dimethoxy-buta-2,3-diyl)-β-D-glucopyranos-1-yl]-benzene

: 1-chloro-2-(4-methoxy-benzyl)-4-[3,4-O-(2,3-dimethoxy-but-2,3-diyl)-β-D-glucopyranos-1-yl]-benzene

Guidance literature:: (2S,3R,4R,5S,6R)-2-(4-chloro-3-(4-methoxybenzyl)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol; dimethylglyoxal; trimethyl orthoformate; With boron trifluoride diethyl etherate; In methanol; at 60 ℃; for 4h;

With triethylamine; In methanol; at 20 ℃; for 0.5h;

Reference yield: 54.0%

: 333359-90-3
(2S,3R,4R,5S,6R)-2-(4-chloro-3-(4-methoxybenzyl)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol

: 431-03-8
dimethylglyoxal

: 149-73-5
trimethyl orthoformate

: 872980-39-7
1-chloro-2-(4-methoxy-benzyl)-4-[2,3-O-(2,3-dimethoxy-buta-2,3-diyl)-β-D-glucopyranos-1-yl]-benzene

: 881636-93-7
C₂₆H₃₃ClO₈

Guidance literature:: With boron trifluoride diethyl etherate; In methanol; at 60 ℃; for 4h;

Reference yield: 64.0%

: 872980-39-7
1-chloro-2-(4-methoxy-benzyl)-4-[2,3-O-(2,3-dimethoxy-buta-2,3-diyl)-β-D-glucopyranos-1-yl]-benzene

: 5-[4-chloro-3-(4-methoxy-benzyl)-phenyl]-8-hydroxy-2,3-dimethoxy-2,3-dimethylhexahydro-pyran[3,4-b][1,4]dioxin-7-carboxylic acid

Guidance literature:: With sodium hypochlorite; tetrabutylammomium bromide; sodium hydrogencarbonate; sodium chloride; potassium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In dichloromethane; water; at 0 ℃; for 4h; Product distribution / selectivity;