3-benzyloxycarbonylaminopropyl 2,3-O-isopropylidene-α-L-rhamnopyranoside

Base Information

Chemical Name:3-benzyloxycarbonylaminopropyl 2,3-O-isopropylidene-α-L-rhamnopyranoside
CAS No.:148404-66-4
Molecular Formula:C₂₀H₂₉NO₇
Molecular Weight:395.453
Hs Code.:

Synonyms:3-benzyloxycarbonylaminopropyl 2,3-O-isopropylidene-α-L-rhamnopyranoside

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Chemical Property of 3-benzyloxycarbonylaminopropyl 2,3-O-isopropylidene-α-L-rhamnopyranoside

Chemical Property:

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Technology Process of 3-benzyloxycarbonylaminopropyl 2,3-O-isopropylidene-α-L-rhamnopyranoside

There total 3 articles about 3-benzyloxycarbonylaminopropyl 2,3-O-isopropylidene-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34637-22-4
3-[(N-benzyloxycarbonyl)amino]propanol

: 148404-66-4
3-benzyloxycarbonylaminopropyl 2,3-O-isopropylidene-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / N-iodosuccinimide, 4 Angstroem molecular sieves / trifluoromethanesulfonic acid / 1,2-dichloro-ethane; diethyl ether / 0.25 h / 0 °C

2: t-BuOK / methanol / 2 h / 20 °C

3: camphorsulfonic acid / acetone / 2 h / 20 °C

With N-iodo-succinimide; 4 A molecular sieve; camphor-10-sulfonic acid; potassium tert-butylate; trifluorormethanesulfonic acid; In methanol; diethyl ether; 1,2-dichloro-ethane; acetone;
DOI:10.1016/0008-6215(93)80102-K

Reference yield:

: 148404-65-3
N-(benzyloxycarbonyl)aminopropyl α-L-rhamnopyranoside

: 77-76-9
2,2-dimethoxy-propane

: 148404-66-4
3-benzyloxycarbonylaminopropyl 2,3-O-isopropylidene-α-L-rhamnopyranoside

Guidance literature:: With camphor-10-sulfonic acid; In acetone; at 20 ℃; for 2h; Yield given;
DOI:10.1016/0008-6215(93)80102-K

Reference yield:

: 148404-64-2
3-benzyloxycarbonylaminopropyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranoside

: 148404-66-4
3-benzyloxycarbonylaminopropyl 2,3-O-isopropylidene-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: t-BuOK / methanol / 2 h / 20 °C

2: camphorsulfonic acid / acetone / 2 h / 20 °C

With camphor-10-sulfonic acid; potassium tert-butylate; In methanol; acetone;
DOI:10.1016/0008-6215(93)80102-K