[Ru(tris(pyrazolyl)borate)(CH₃NHNH₂)(P(OEt)2Ph)(PPh₃)](BPh₄)

Base Information

• Chemical Name: [Ru(tris(pyrazolyl)borate)(CH₃NHNH₂)(P(OEt)2Ph)(PPh₃)](BPh₄)
• CAS No.: 736929-42-3
• Molecular Formula: C₂₄H₂₀B*C₃₈H₄₆BN₈O₂P₂Ru
• Molecular Weight: 1139.9
• Mol file: 736929-42-3.mol

Synonyms:[Ru(tris(pyrazolyl)borate)(CH₃NHNH₂)(P(OEt)2Ph)(PPh₃)](BPh₄)

Chemical Property of [Ru(tris(pyrazolyl)borate)(CH₃NHNH₂)(P(OEt)2Ph)(PPh₃)](BPh₄)

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of [Ru(tris(pyrazolyl)borate)(CH₃NHNH₂)(P(OEt)2Ph)(PPh₃)](BPh₄)

There total 1 articles about [Ru(tris(pyrazolyl)borate)(CH₃NHNH₂)(P(OEt)2Ph)(PPh₃)](BPh₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

[Ru(tris(pyrazolyl)borate)(H)(P(OEt)3)(P(OEt)2C6H5)] (736929-70-7) + sodium tetraphenyl borate (143-66-8) + methylhydrazine (60-34-4) → [Ru(tris(pyrazolyl)borate)(CH3NHNH2)(P(OEt)2Ph)(PPh3)](BPh4) (736929-42-3)

Guidance literature:

With CF₃SO₃H; In dichloromethane; to a soln. of complex in CH2Cl2 cooled to -196°C was added an equiv of CF3SO3H, the mixt. was brought to 0°C and stirred for 30 min, an excess of hydrazine was added, stirred for 2 h; evapd., tritured with ethanol containing NaBPh4, the solid was filtered,crystd. from CH2Cl2 and ethanol; elem. anal.;

DOI:10.1021/ic0497275

upstream raw materials:

[Ru(tris(pyrazolyl)borate)(H)(P(OEt)3)(P(OEt)2C₆H₅)]

sodium tetraphenyl borate

methylhydrazine