(+)-(1S,2S)-2-((R)-2-((R)-4-methylcyclohex-3-en-1-yl)propyl)cyclopentyl acetate

Base Information

Chemical Name:(+)-(1S,2S)-2-((R)-2-((R)-4-methylcyclohex-3-en-1-yl)propyl)cyclopentyl acetate
CAS No.:1456882-25-9
Molecular Formula:C₁₇H₂₈O₂
Molecular Weight:264.408
Hs Code.:

Synonyms:(+)-(1S,2S)-2-((R)-2-((R)-4-methylcyclohex-3-en-1-yl)propyl)cyclopentyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-(1S,2S)-2-((R)-2-((R)-4-methylcyclohex-3-en-1-yl)propyl)cyclopentyl acetate

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Technology Process of (+)-(1S,2S)-2-((R)-2-((R)-4-methylcyclohex-3-en-1-yl)propyl)cyclopentyl acetate

There total 3 articles about (+)-(1S,2S)-2-((R)-2-((R)-4-methylcyclohex-3-en-1-yl)propyl)cyclopentyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1035967-90-8
(+)-(1S,2S)-2-((R)-2-((R)-4-methylcyclohex-3-en-1-yl)propyl)cyclopentanol

: 108-24-7
acetic anhydride

: 1456882-25-9
(+)-(1S,2S)-2-((R)-2-((R)-4-methylcyclohex-3-en-1-yl)propyl)cyclopentyl acetate

Guidance literature:: With pyridine; dmap; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja407388y

Reference yield:

: 1035968-04-7
(+)-Nectaryl(R)

: 1456882-25-9
(+)-(1S,2S)-2-((R)-2-((R)-4-methylcyclohex-3-en-1-yl)propyl)cyclopentyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: L-Selectride / tetrahydrofuran / 3 h / -78 - 20 °C / Inert atmosphere

2: pyridine; dmap / dichloromethane / 12 h / 20 °C / Inert atmosphere

With pyridine; dmap; L-Selectride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja407388y

Reference yield:

: C₁₅H₂₆O

: 1456882-25-9
(+)-(1S,2S)-2-((R)-2-((R)-4-methylcyclohex-3-en-1-yl)propyl)cyclopentyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: Amano Lipase PS / tert-butyl methyl ether / Inert atmosphere

2: pyridine; dmap / dichloromethane / 12 h / 20 °C / Inert atmosphere

With pyridine; dmap; Amano Lipase PS; In dichloromethane; tert-butyl methyl ether;
DOI:10.1021/ja407388y