(+)-(1S,2S)-2-((R)-2-((1r,4R)-4-methylcyclohexyl)propyl)cyclopentyl acetate

Base Information

Chemical Name:(+)-(1S,2S)-2-((R)-2-((1r,4R)-4-methylcyclohexyl)propyl)cyclopentyl acetate
CAS No.:1456882-26-0
Molecular Formula:C₁₇H₃₀O₂
Molecular Weight:266.424
Hs Code.:

Synonyms:(+)-(1S,2S)-2-((R)-2-((1r,4R)-4-methylcyclohexyl)propyl)cyclopentyl acetate

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Chemical Property of (+)-(1S,2S)-2-((R)-2-((1r,4R)-4-methylcyclohexyl)propyl)cyclopentyl acetate

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Technology Process of (+)-(1S,2S)-2-((R)-2-((1r,4R)-4-methylcyclohexyl)propyl)cyclopentyl acetate

There total 4 articles about (+)-(1S,2S)-2-((R)-2-((1r,4R)-4-methylcyclohexyl)propyl)cyclopentyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1456882-25-9
(+)-(1S,2S)-2-((R)-2-((R)-4-methylcyclohex-3-en-1-yl)propyl)cyclopentyl acetate

: 1456882-26-0
(+)-(1S,2S)-2-((R)-2-((1r,4R)-4-methylcyclohexyl)propyl)cyclopentyl acetate

Guidance literature:: With (+)-(R)-[1,5-cycloocatdien-7-(2-phenyl-6,7-dihydro-5H-[1]pyridine)-di-(tert-butyl)phosphinite-ridiumd(I)]tetrakis-(3,5-bis(trifluoromethyl)phenyl)borate; hydrogen; In dichloromethane; at 20 ℃; for 5h; under 25858.1 Torr; Inert atmosphere;
DOI:10.1021/ja407388y

Reference yield:

: 1035968-04-7
(+)-Nectaryl(R)

: 1456882-26-0
(+)-(1S,2S)-2-((R)-2-((1r,4R)-4-methylcyclohexyl)propyl)cyclopentyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: L-Selectride / tetrahydrofuran / 3 h / -78 - 20 °C / Inert atmosphere

2: pyridine; dmap / dichloromethane / 12 h / 20 °C / Inert atmosphere

3: (+)-(R)-[1,5-cycloocatdien-7-(2-phenyl-6,7-dihydro-5H-[1]pyridine)-di-(tert-butyl)phosphinite-ridiumd(I)]tetrakis-(3,5-bis(trifluoromethyl)phenyl)borate; hydrogen / dichloromethane / 5 h / 20 °C / 25858.1 Torr / Inert atmosphere

With pyridine; dmap; (+)-(R)-[1,5-cycloocatdien-7-(2-phenyl-6,7-dihydro-5H-[1]pyridine)-di-(tert-butyl)phosphinite-ridiumd(I)]tetrakis-(3,5-bis(trifluoromethyl)phenyl)borate; hydrogen; L-Selectride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja407388y

Reference yield:

: 1035967-90-8
(+)-(1S,2S)-2-((R)-2-((R)-4-methylcyclohex-3-en-1-yl)propyl)cyclopentanol

: 1456882-26-0
(+)-(1S,2S)-2-((R)-2-((1r,4R)-4-methylcyclohexyl)propyl)cyclopentyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; dmap / dichloromethane / 12 h / 20 °C / Inert atmosphere

2: (+)-(R)-[1,5-cycloocatdien-7-(2-phenyl-6,7-dihydro-5H-[1]pyridine)-di-(tert-butyl)phosphinite-ridiumd(I)]tetrakis-(3,5-bis(trifluoromethyl)phenyl)borate; hydrogen / dichloromethane / 5 h / 20 °C / 25858.1 Torr / Inert atmosphere

With pyridine; dmap; (+)-(R)-[1,5-cycloocatdien-7-(2-phenyl-6,7-dihydro-5H-[1]pyridine)-di-(tert-butyl)phosphinite-ridiumd(I)]tetrakis-(3,5-bis(trifluoromethyl)phenyl)borate; hydrogen; In dichloromethane;
DOI:10.1021/ja407388y