9-[2-deoxy-3,5-di-O-(4-methylbenzoyl)-β-D-erythropentofuranosyl]-6-fluoropurine

Base Information

Chemical Name:9-[2-deoxy-3,5-di-O-(4-methylbenzoyl)-β-D-erythropentofuranosyl]-6-fluoropurine
CAS No.:849936-57-8
Molecular Formula:C₂₆H₂₃FN₄O₅
Molecular Weight:490.491
Hs Code.:

Synonyms:9-[2-deoxy-3,5-di-O-(4-methylbenzoyl)-β-D-erythropentofuranosyl]-6-fluoropurine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-[2-deoxy-3,5-di-O-(4-methylbenzoyl)-β-D-erythropentofuranosyl]-6-fluoropurine

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Technology Process of 9-[2-deoxy-3,5-di-O-(4-methylbenzoyl)-β-D-erythropentofuranosyl]-6-fluoropurine

There total 1 articles about 9-[2-deoxy-3,5-di-O-(4-methylbenzoyl)-β-D-erythropentofuranosyl]-6-fluoropurine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 121409-45-8
2'-deoxy-3',5'-di-O-(4-methylbenzoyl)adenosine

: 849936-57-8
9-[2-deoxy-3,5-di-O-(4-methylbenzoyl)-β-D-erythropentofuranosyl]-6-fluoropurine

Guidance literature:: With tert.-butylnitrite; pyridine hydrogenfluoride; at -15 ℃; for 0.25h;
DOI:10.1021/ol050063s

Reference yield: 67.0%

: 849936-57-8
9-[2-deoxy-3,5-di-O-(4-methylbenzoyl)-β-D-erythropentofuranosyl]-6-fluoropurine

: 1765-93-1
4-fluoroboronic acid

: 328378-38-7
9-[2-deoxy-3,5-di-O-(4-methylbenzoyl)-β-D-erythro-pentofuranosyl]-6-(4-fluorophenyl)purine

Guidance literature:: With potassium phosphate; 1,3-bis(2,6-diisopropylphenyl)imidazolidin-2-ylidene hydrochloride; bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; In tetrahydrofuran; at 60 ℃; for 3h;
DOI:10.1021/ol050063s

Reference yield: 60.0%

: 849936-57-8
9-[2-deoxy-3,5-di-O-(4-methylbenzoyl)-β-D-erythropentofuranosyl]-6-fluoropurine

: 5720-05-8
4-methylphenylboronic acid

: 9-[2-deoxy-3,5-di-O-(4-methylbenzoyl)-β-D-erythro-pentofuranosyl]-6-(4-methylphenyl)purine

Guidance literature:: With potassium phosphate; 1,3-bis(2,6-diisopropylphenyl)imidazolidin-2-ylidene hydrochloride; bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; In tetrahydrofuran; at 60 ℃; for 3h;
DOI:10.1021/ol050063s