(S)-6-methyl-3-(4,4,6-trimethyl-1,3,2-dioxaborato)heptanoic acid phenyl amide

Base Information

Chemical Name:(S)-6-methyl-3-(4,4,6-trimethyl-1,3,2-dioxaborato)heptanoic acid phenyl amide
CAS No.:1415610-11-5
Molecular Formula:C₂₀H₃₂BNO₃
Molecular Weight:345.29
Hs Code.:

Synonyms:(S)-6-methyl-3-(4,4,6-trimethyl-1,3,2-dioxaborato)heptanoic acid phenyl amide

Suppliers and Price of (S)-6-methyl-3-(4,4,6-trimethyl-1,3,2-dioxaborato)heptanoic acid phenyl amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-6-methyl-3-(4,4,6-trimethyl-1,3,2-dioxaborato)heptanoic acid phenyl amide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-6-methyl-3-(4,4,6-trimethyl-1,3,2-dioxaborato)heptanoic acid phenyl amide

There total 4 articles about (S)-6-methyl-3-(4,4,6-trimethyl-1,3,2-dioxaborato)heptanoic acid phenyl amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1016225-09-4
(E)-6-methyl-3-heptenoic acid phenyl amide

: 10199-14-1,23894-82-8
4,4,6-trimethyl-1,3,2-dioxaborinane

: 1415610-11-5
(S)-6-methyl-3-(4,4,6-trimethyl-1,3,2-dioxaborato)heptanoic acid phenyl amide

Guidance literature:: With bis(norbornadiene)rhodium(l)tetrafluoroborate; (R)-2-(2,3,4,5-tetrahydrobenzo[b]oxepin-3-yl)acetic acid tert-butyl ester; In tetrahydrofuran; at 40 ℃;
DOI:10.1039/c2cc36199j

Reference yield:

: 1016225-27-6,168213-35-2
(E)-6-methylhept-3-enoic acid

: 1415610-11-5
(S)-6-methyl-3-(4,4,6-trimethyl-1,3,2-dioxaborato)heptanoic acid phenyl amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-dimethyl-formamide / 5 h / 0 °C

1.2: 0 - 20 °C

2.1: bis(norbornadiene)rhodium(l)tetrafluoroborate; (R)-2-(2,3,4,5-tetrahydrobenzo[b]oxepin-3-yl)acetic acid tert-butyl ester / tetrahydrofuran / 40 °C

With bis(norbornadiene)rhodium(l)tetrafluoroborate; (R)-2-(2,3,4,5-tetrahydrobenzo[b]oxepin-3-yl)acetic acid tert-butyl ester; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c2cc36199j

Reference yield:

: 62-53-3
aniline

: 1415610-11-5
(S)-6-methyl-3-(4,4,6-trimethyl-1,3,2-dioxaborato)heptanoic acid phenyl amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-dimethyl-formamide / 5 h / 0 °C

1.2: 0 - 20 °C

2.1: bis(norbornadiene)rhodium(l)tetrafluoroborate; (R)-2-(2,3,4,5-tetrahydrobenzo[b]oxepin-3-yl)acetic acid tert-butyl ester / tetrahydrofuran / 40 °C

With bis(norbornadiene)rhodium(l)tetrafluoroborate; (R)-2-(2,3,4,5-tetrahydrobenzo[b]oxepin-3-yl)acetic acid tert-butyl ester; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c2cc36199j