(S)-3-hydroxy-6-methylheptanoic acid phenyl amide

Base Information

Chemical Name:(S)-3-hydroxy-6-methylheptanoic acid phenyl amide
CAS No.:1016225-16-3
Molecular Formula:C₁₄H₂₁NO₂
Molecular Weight:235.326
Hs Code.:

Synonyms:(S)-3-hydroxy-6-methylheptanoic acid phenyl amide

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Chemical Property of (S)-3-hydroxy-6-methylheptanoic acid phenyl amide

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Technology Process of (S)-3-hydroxy-6-methylheptanoic acid phenyl amide

There total 4 articles about (S)-3-hydroxy-6-methylheptanoic acid phenyl amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1415610-11-5
(S)-6-methyl-3-(4,4,6-trimethyl-1,3,2-dioxaborato)heptanoic acid phenyl amide

: 1016225-16-3
(S)-3-hydroxy-6-methylheptanoic acid phenyl amide

Guidance literature:: With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; for 2h;
DOI:10.1039/c2cc36199j

Reference yield:

: 1016225-09-4
(E)-6-methyl-3-heptenoic acid phenyl amide

: 3-hydroxy-6-methyl-N-phenylheptanamide

: 1016225-16-3
(S)-3-hydroxy-6-methylheptanoic acid phenyl amide

: 4658-74-6
4-Hydroxy-6-methyl-heptan-1-saeure-anilid

Guidance literature:: (E)-6-methyl-3-heptenoic acid phenyl amide; With Pinacolborane; di(norbornadiene)rhodium(I) tetrafluoroborate; In tetrahydrofuran; at 40 ℃; for 12h;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; methanol; at 0 - 20 ℃; for 2h; Further stages. Title compound not separated from byproducts.;
DOI:10.1021/ja710492q

Reference yield:

: 62-53-3
aniline

: 1016225-16-3
(S)-3-hydroxy-6-methylheptanoic acid phenyl amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: N,N-dimethyl-formamide / 5 h / 0 °C

1.2: 0 - 20 °C

2.1: bis(norbornadiene)rhodium(l)tetrafluoroborate; (R)-2-(2,3,4,5-tetrahydrobenzo[b]oxepin-3-yl)acetic acid tert-butyl ester / tetrahydrofuran / 40 °C

3.1: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h

With bis(norbornadiene)rhodium(l)tetrafluoroborate; (R)-2-(2,3,4,5-tetrahydrobenzo[b]oxepin-3-yl)acetic acid tert-butyl ester; dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1039/c2cc36199j