(2R,5S)-2-<(Benzyloxy)methyl>-5-<(tert-butyldiphenylsiloxy)methyl>tetrahydrofuran

Base Information

Chemical Name:(2R,5S)-2-<(Benzyloxy)methyl>-5-<(tert-butyldiphenylsiloxy)methyl>tetrahydrofuran
CAS No.:170305-53-0
Molecular Formula:C₂₉H₃₆O₃Si
Molecular Weight:460.689
Hs Code.:

Synonyms:(2R,5S)-2-<(Benzyloxy)methyl>-5-<(tert-butyldiphenylsiloxy)methyl>tetrahydrofuran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,5S)-2-<(Benzyloxy)methyl>-5-<(tert-butyldiphenylsiloxy)methyl>tetrahydrofuran

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Technology Process of (2R,5S)-2-<(Benzyloxy)methyl>-5-<(tert-butyldiphenylsiloxy)methyl>tetrahydrofuran

There total 1 articles about (2R,5S)-2-<(Benzyloxy)methyl>-5-<(tert-butyldiphenylsiloxy)methyl>tetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 100-39-0
benzyl bromide

: 165449-97-8
(2R,5S)-5-<(tert-butyldiphenylsiloxy)methyl>tetrahydrofuran-2-methanol

: 170305-53-0
(2R,5S)-2-<(Benzyloxy)methyl>-5-<(tert-butyldiphenylsiloxy)methyl>tetrahydrofuran

Guidance literature:: With sodium hydride; 1.) DMF, 15 min, 2.) THF, r.t., 10 h;

Reference yield: 95.0%

: 170305-53-0
(2R,5S)-2-<(Benzyloxy)methyl>-5-<(tert-butyldiphenylsiloxy)methyl>tetrahydrofuran

: 158110-03-3
(2S,5R)-5-<(Benzyloxy)methyl>tetrahydrofuran-2-methanol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 3h; Ambient temperature;

Reference yield:

: 170305-53-0
(2R,5S)-2-<(Benzyloxy)methyl>-5-<(tert-butyldiphenylsiloxy)methyl>tetrahydrofuran

: 170305-54-1
(2S,5R)-5-<(Benzyloxy)methyl>tetrahydrofuran-2-carboxaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / n-Bu₄NF*H₂O / tetrahydrofuran / 3 h / Ambient temperature

2: 1.) (COCl)2, DMSO, 2.) Et₃N / 1.) CH₂Cl₂, -78 deg C, 15 min, 2.) -78 to 0 deg C, 30 min

With oxalyl dichloride; tetrabutyl ammonium fluoride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran;