C₂₇H₂₈N₄O₃S₂

Base Information

Chemical Name:C₂₇H₂₈N₄O₃S₂
CAS No.:1447194-80-0
Molecular Formula:C₂₇H₂₈N₄O₃S₂
Molecular Weight:520.676
Hs Code.:

C<sub>27</sub>H<sub>28</sub>N<sub>4</sub>O<sub>3</sub>S<sub>2</sub>

Synonyms:C₂₇H₂₈N₄O₃S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₂₈N₄O₃S₂

Chemical Property:

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Technology Process of C₂₇H₂₈N₄O₃S₂

There total 13 articles about C₂₇H₂₈N₄O₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1447195-24-5
C₄₂H₃₈N₄O₅S₂

: 1447194-80-0
C₂₇H₂₈N₄O₃S₂

Guidance literature:: With diethylamine; In d₇-N,N-dimethylformamide; at 20 ℃; for 0.5h;
DOI:10.1002/anie.201302106

Reference yield:

: 1447194-67-3
benzyl (4S)-4-(N-fmoc)-amino-3-oxopentanoate

: 1447194-80-0
C₂₇H₂₈N₄O₃S₂

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuryl dichloride / dichloromethane / 1 h / 0 - 20 °C

2: ethanol / 40 °C

3: hydrogen; rosenmund catalyst / tetrahydrofuran; ethanol / 30 °C

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 4.5 h / 0 - 20 °C

5: diethylamine / d₇-N,N-dimethylformamide / 0.5 h / 20 °C

With sulfuryl dichloride; rosenmund catalyst; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; In tetrahydrofuran; ethanol; dichloromethane; d₇-N,N-dimethylformamide;
DOI:10.1002/anie.201302106

Reference yield:

: 35661-40-6
N-Fmoc L-Phe

: 1447194-80-0
C₂₇H₂₈N₄O₃S₂

Guidance literature:: Multi-step reaction with 8 steps

1: hydrogenchloride; 4-methyl-morpholine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / dichloromethane

2: lithium aluminium tetrahydride / tetrahydrofuran / -25 °C

3: tin(ll) chloride / dichloromethane

4: sulfuryl dichloride / dichloromethane / 1 h / 0 - 20 °C

5: ethanol / 40 °C

6: d₇-N,N-dimethylformamide; diethylamine / 0.5 h / 20 °C

7: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 4.5 h / 0 - 20 °C

8: diethylamine / d₇-N,N-dimethylformamide / 0.5 h / 20 °C

With 4-methyl-morpholine; hydrogenchloride; lithium aluminium tetrahydride; sulfuryl dichloride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; tin(ll) chloride; In tetrahydrofuran; ethanol; dichloromethane; d₇-N,N-dimethylformamide; diethylamine;
DOI:10.1002/anie.201302106