3-benzyl-α-chloropropiophenone

Base Information

Chemical Name:3-benzyl-α-chloropropiophenone
CAS No.:259878-87-0
Molecular Formula:C₁₆H₁₅ClO
Molecular Weight:258.748
Hs Code.:

Synonyms:3-benzyl-α-chloropropiophenone

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Chemical Property of 3-benzyl-α-chloropropiophenone

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Technology Process of 3-benzyl-α-chloropropiophenone

There total 4 articles about 3-benzyl-α-chloropropiophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 7623-09-8
2-chloropropionyl chloride

: 27798-39-6
1-benzyl-3-bromobenzene

: 259878-87-0
3-benzyl-α-chloropropiophenone

Guidance literature:: 1-benzyl-3-bromobenzene; With iodine; magnesium; In tetrahydrofuran; for 3h; Heating;

2-chloropropionyl chloride; With iron(III)-acetylacetonate; In tetrahydrofuran; at 20 ℃; for 0.25h;

Reference yield:

: 1711-09-7
3-bromobenzoyl chloride

: 259878-87-0
3-benzyl-α-chloropropiophenone

Guidance literature:: Multi-step reaction with 3 steps

1.1: 72.85 g / AlCl₃ / 20 °C

2.1: 93.5 percent / hydrazine hydrate; KOH / ethane-1,2-diol / 9.5 h / 155 - 198 °C

3.1: magnesium; iodine / tetrahydrofuran / 3 h / Heating

3.2: 88 percent / tris(acetylacetonate)iron / tetrahydrofuran / 0.25 h / 20 °C

With potassium hydroxide; aluminium trichloride; iodine; hydrazine hydrate; magnesium; In tetrahydrofuran; ethylene glycol; 1.1: Friedel-Crafts acylation / 2.1: Reduction / 3.1: Metallation / 3.2: Grignard reaction;

Reference yield:

: 585-76-2
m-bromobenzoic acid

: 259878-87-0
3-benzyl-α-chloropropiophenone

Guidance literature:: Multi-step reaction with 4 steps

1.1: PCl₅ / benzene / 2 h / Heating

2.1: 72.85 g / AlCl₃ / 20 °C

3.1: 93.5 percent / hydrazine hydrate; KOH / ethane-1,2-diol / 9.5 h / 155 - 198 °C

4.1: magnesium; iodine / tetrahydrofuran / 3 h / Heating

4.2: 88 percent / tris(acetylacetonate)iron / tetrahydrofuran / 0.25 h / 20 °C

With potassium hydroxide; aluminium trichloride; phosphorus pentachloride; iodine; hydrazine hydrate; magnesium; In tetrahydrofuran; ethylene glycol; benzene; 1.1: Substitution / 2.1: Friedel-Crafts acylation / 3.1: Reduction / 4.1: Metallation / 4.2: Grignard reaction;